1-(2-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-thienyl)-2-(3-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-2-thienyl)hexafluorocyclopentene

Base Information

• Chemical Name: 1-(2-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-thienyl)-2-(3-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-2-thienyl)hexafluorocyclopentene
• CAS No.: 817180-75-9
• Molecular Formula: C₆₁H₆₈F₈O₂S₂
• Molecular Weight: 1049.33

Synonyms:1-(2-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-thienyl)-2-(3-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-2-thienyl)hexafluorocyclopentene

Chemical Property of 1-(2-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-thienyl)-2-(3-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-2-thienyl)hexafluorocyclopentene

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Technology Process of 1-(2-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-thienyl)-2-(3-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-2-thienyl)hexafluorocyclopentene

There total 2 articles about 1-(2-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-thienyl)-2-(3-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-2-thienyl)hexafluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

2-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-4-methylthiophene + 5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-(2,3,3,4,4,5,5-heptafluorocyclopent-1-enyl)-2-methylthiophene → 1-(2-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-thienyl)-2-(3-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-2-thienyl)hexafluorocyclopentene (817180-75-9)

Guidance literature:

2-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-4-methylthiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -30 ℃; for 1h;

5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-(2,3,3,4,4,5,5-heptafluorocyclopent-1-enyl)-2-methylthiophene; In tetrahydrofuran; hexane; at -78 - 20 ℃;

DOI:10.1021/ja0468269

Reference yield:

(3aR,3bR)-7,7,8,8,9,9-Hexafluoro-2,5-bis-(2-fluoro-4'-undecyloxy-biphenyl-4-yl)-3a,3b-dimethyl-3a,7,8,9-tetrahydro-3bH-1,4-dithia-trindene → 1-(2-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-thienyl)-2-(3-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-2-thienyl)hexafluorocyclopentene (817180-75-9)

Guidance literature:

In cyclohexane; at 25 ℃; Quantum yield; visible-light irradiation;

DOI:10.1021/ja0468269

Reference yield:

1-(2-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-3-thienyl)-2-(3-methyl-5-(2-fluoro-4'-undecyloxybiphenyl-4-yl)-2-thienyl)hexafluorocyclopentene (817180-75-9) → (3aR,3bR)-7,7,8,8,9,9-Hexafluoro-2,5-bis-(2-fluoro-4'-undecyloxy-biphenyl-4-yl)-3a,3b-dimethyl-3a,7,8,9-tetrahydro-3bH-1,4-dithia-trindene

Guidance literature:

In cyclohexane; at 25 ℃; Quantum yield; UV-irradiation;

DOI:10.1021/ja0468269

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