1-hexyl-3-methyl-4-phenyl-1H-1,2,3-triazol-3-ium bis[(trifluoromethyl)sulfonyl]amide

Base Information

Chemical Name:1-hexyl-3-methyl-4-phenyl-1H-1,2,3-triazol-3-ium bis[(trifluoromethyl)sulfonyl]amide
CAS No.:1352807-75-0
Molecular Formula:C₂F₆NO₄S₂*C₁₅H₂₂N₃
Molecular Weight:524.508
Hs Code.:

Synonyms:1-hexyl-3-methyl-4-phenyl-1H-1,2,3-triazol-3-ium bis[(trifluoromethyl)sulfonyl]amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-hexyl-3-methyl-4-phenyl-1H-1,2,3-triazol-3-ium bis[(trifluoromethyl)sulfonyl]amide

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Technology Process of 1-hexyl-3-methyl-4-phenyl-1H-1,2,3-triazol-3-ium bis[(trifluoromethyl)sulfonyl]amide

There total 5 articles about 1-hexyl-3-methyl-4-phenyl-1H-1,2,3-triazol-3-ium bis[(trifluoromethyl)sulfonyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1352807-60-3
1-hexyl-3-methyl-4-phenyl-1H-1,2,3-triazol-3-ium iodide

: 90076-65-6
bis(trifluoromethane)sulfonimide lithium

: 1352807-75-0
1-hexyl-3-methyl-4-phenyl-1H-1,2,3-triazol-3-ium bis[(trifluoromethyl)sulfonyl]amide

Guidance literature:: DOI:10.1039/c1gc16067b

Reference yield:

: 6926-45-0
1-azidohexane

: 1352807-75-0
1-hexyl-3-methyl-4-phenyl-1H-1,2,3-triazol-3-ium bis[(trifluoromethyl)sulfonyl]amide

Guidance literature:: Multi-step reaction with 3 steps

1: copper(II) sulfate; sodium L-ascorbate / water; butan-1-ol / 24 h / 20 °C

2: acetonitrile / 12 h / Reflux

With copper(II) sulfate; sodium L-ascorbate; In water; acetonitrile; butan-1-ol;
DOI:10.1039/c1gc16067b

Reference yield:

: 111-25-1
1-bromo-hexane

: 1352807-75-0
1-hexyl-3-methyl-4-phenyl-1H-1,2,3-triazol-3-ium bis[(trifluoromethyl)sulfonyl]amide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide / N,N-dimethyl-formamide / 24 h / 20 °C

2: copper(II) sulfate; sodium L-ascorbate / water; butan-1-ol / 24 h / 20 °C

3: acetonitrile / 12 h / Reflux

With sodium azide; copper(II) sulfate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; acetonitrile; butan-1-ol;
DOI:10.1039/c1gc16067b