C₃₇H₇₂N₄O₃SSi₃

Base Information

Chemical Name:C₃₇H₇₂N₄O₃SSi₃
CAS No.:1349054-48-3
Molecular Formula:C₃₇H₇₂N₄O₃SSi₃
Molecular Weight:737.326
Hs Code.:

C<sub>37</sub>H<sub>72</sub>N<sub>4</sub>O<sub>3</sub>SSi<sub>3</sub>

Synonyms:C₃₇H₇₂N₄O₃SSi₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₇₂N₄O₃SSi₃

Chemical Property:

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Technology Process of C₃₇H₇₂N₄O₃SSi₃

There total 18 articles about C₃₇H₇₂N₄O₃SSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1349054-10-9
C₂₈H₅₂N₄O₃SSi₂

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1349054-48-3
C₃₇H₇₂N₄O₃SSi₃

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -73 - -60 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol2024746

Reference yield:

: C₁₄H₁₈O₃S

: 1349054-48-3
C₃₇H₇₂N₄O₃SSi₃

Guidance literature:: Multi-step reaction with 16 steps

1.1: tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 4.17 h / 25 °C

2.1: 1H-imidazole / 1,2-dichloro-ethane / 0 - 25 °C / Inert atmosphere

3.1: trimethylaluminum; N-ethyl-N,N-diisopropylamine / hexane; dichloromethane / 2 h / -78 - 25 °C / Inert atmosphere

4.1: toluene / 0.25 h / 0 °C

4.2: 0.08 h / 0 °C

4.3: 20 °C

5.1: dichloromethane / 0.17 h / 0 °C / Inert atmosphere

5.2: 2 h / 0 °C / Inert atmosphere

6.1: toluene / 1 h / 50 - 60 °C

7.1: tetrahydrofuran; toluene / 25 °C / Inert atmosphere

8.1: dichloromethane / 0.25 h / 0 °C

8.2: 0 °C

9.1: methanol / 0.5 h

9.2: 2 h / 0 °C

10.1: ozone / ethyl acetate / 0.5 h / 40 °C

10.2: 8 h / 20 °C / Inert atmosphere

10.3: 0.5 h / Inert atmosphere

11.1: bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; triphenylphosphine / dichloromethane / 1.5 h / Inert atmosphere

12.1: isopropylmagnesium chloride / tetrahydrofuran / 2 h / -15 - -10 °C / Inert atmosphere

13.1: 1H-imidazole / 1,2-dichloro-ethane / 6 h / 0 - 80 °C / Inert atmosphere

14.1: diisobutylaluminium hydride / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

15.1: borane tert-butylamine / ethanol / 1 h / -78 - 25 °C

15.2: 0 °C

16.1: 2,6-dimethylpyridine / dichloromethane / 4 h / -73 - -60 °C / Inert atmosphere

With 1H-imidazole; bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; 2,6-dimethylpyridine; methanol; trimethylaluminum; isopropylmagnesium chloride; diisobutylaluminium hydride; borane tert-butylamine; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; toluene; 4.1: Noyori oxidation / 4.2: Noyori oxidation / 4.3: Noyori oxidation / 5.1: Jacobsen epoxidation / 5.2: Jacobsen epoxidation;
DOI:10.1021/ol2024746

Reference yield:

: 1349053-72-0
C₂₆H₃₆O₃S₂Si

: 1349054-48-3
C₃₇H₇₂N₄O₃SSi₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: trimethylaluminum; N-ethyl-N,N-diisopropylamine / hexane; dichloromethane / 2 h / -78 - 25 °C / Inert atmosphere

2.1: toluene / 0.25 h / 0 °C

2.2: 0.08 h / 0 °C

2.3: 20 °C

3.1: dichloromethane / 0.17 h / 0 °C / Inert atmosphere

3.2: 2 h / 0 °C / Inert atmosphere

4.1: toluene / 1 h / 50 - 60 °C

5.1: tetrahydrofuran; toluene / 25 °C / Inert atmosphere

6.1: dichloromethane / 0.25 h / 0 °C

6.2: 0 °C

7.1: methanol / 0.5 h

7.2: 2 h / 0 °C

8.1: ozone / ethyl acetate / 0.5 h / 40 °C

8.2: 8 h / 20 °C / Inert atmosphere

8.3: 0.5 h / Inert atmosphere

9.1: bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; triphenylphosphine / dichloromethane / 1.5 h / Inert atmosphere

10.1: isopropylmagnesium chloride / tetrahydrofuran / 2 h / -15 - -10 °C / Inert atmosphere

11.1: 1H-imidazole / 1,2-dichloro-ethane / 6 h / 0 - 80 °C / Inert atmosphere

12.1: diisobutylaluminium hydride / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

13.1: borane tert-butylamine / ethanol / 1 h / -78 - 25 °C

13.2: 0 °C

14.1: 2,6-dimethylpyridine / dichloromethane / 4 h / -73 - -60 °C / Inert atmosphere

With 1H-imidazole; bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; 2,6-dimethylpyridine; methanol; trimethylaluminum; isopropylmagnesium chloride; diisobutylaluminium hydride; borane tert-butylamine; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; toluene; 2.1: Noyori oxidation / 2.2: Noyori oxidation / 2.3: Noyori oxidation / 3.1: Jacobsen epoxidation / 3.2: Jacobsen epoxidation;
DOI:10.1021/ol2024746