2(S)-2-(benzyloxycarbonylamino)-6-iodocaproic acid benzyl ester

Base Information

Chemical Name:2(S)-2-(benzyloxycarbonylamino)-6-iodocaproic acid benzyl ester
CAS No.:169059-74-9
Molecular Formula:C₂₁H₂₄INO₄
Molecular Weight:481.33
Hs Code.:

Synonyms:2(S)-2-(benzyloxycarbonylamino)-6-iodocaproic acid benzyl ester

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Chemical Property of 2(S)-2-(benzyloxycarbonylamino)-6-iodocaproic acid benzyl ester

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Technology Process of 2(S)-2-(benzyloxycarbonylamino)-6-iodocaproic acid benzyl ester

There total 4 articles about 2(S)-2-(benzyloxycarbonylamino)-6-iodocaproic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2(S)-2-(benzyloxycarbonylamino)-6-mesyloxycaproic acid benzyl ester

: 169059-74-9
2(S)-2-(benzyloxycarbonylamino)-6-iodocaproic acid benzyl ester

Guidance literature:: With sodium iodide; In acetone; for 5h; Heating;
DOI:10.1002/ardp.19953280414

Reference yield:

: 84246-49-1
2(S)-2-(benzyloxycarbonylamino)-6-hydroxyhexanoic acid, benzyl ester

: 169059-74-9
2(S)-2-(benzyloxycarbonylamino)-6-iodocaproic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane

2: sodium iodide / acetone

With pyridine; sodium iodide; In dichloromethane; acetone;
DOI:10.1021/jm400792m

Reference yield:

: 2212-75-1
N₂-[(benzyloxy)carbonyl]-L-lysine

: 169059-74-9
2(S)-2-(benzyloxycarbonylamino)-6-iodocaproic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; sodium nitroprusside / water / 60 °C

2: triethylamine / acetone

3: pyridine / dichloromethane

4: sodium iodide / acetone

With pyridine; sodium nitroprusside; triethylamine; sodium iodide; sodium hydroxide; In dichloromethane; water; acetone;
DOI:10.1021/jm400792m