[4-(4-chlorophenyl)-1-(3-methyl-2-butenyl)-1H-pyrrol-3-yl]phenylmethanone

Base Information

Chemical Name:[4-(4-chlorophenyl)-1-(3-methyl-2-butenyl)-1H-pyrrol-3-yl]phenylmethanone
CAS No.:863097-41-0
Molecular Formula:C₂₂H₂₀ClNO
Molecular Weight:349.86
Hs Code.:

Synonyms:[4-(4-chlorophenyl)-1-(3-methyl-2-butenyl)-1H-pyrrol-3-yl]phenylmethanone

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Chemical Property of [4-(4-chlorophenyl)-1-(3-methyl-2-butenyl)-1H-pyrrol-3-yl]phenylmethanone

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Technology Process of [4-(4-chlorophenyl)-1-(3-methyl-2-butenyl)-1H-pyrrol-3-yl]phenylmethanone

There total 1 articles about [4-(4-chlorophenyl)-1-(3-methyl-2-butenyl)-1H-pyrrol-3-yl]phenylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 870-63-3
prenyl bromide

: 150061-84-0
(4-(4-chlorophenyl)-1H-pyrrol-3-yl)(phenyl)methanone

: 863097-41-0
[4-(4-chlorophenyl)-1-(3-methyl-2-butenyl)-1H-pyrrol-3-yl]phenylmethanone

Guidance literature:: (4-(4-chlorophenyl)-1H-pyrrol-3-yl)(phenyl)methanone; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.166667h;

prenyl bromide; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1021/jm048997u

Reference yield: 92.0%

: 863097-41-0
[4-(4-chlorophenyl)-1-(3-methyl-2-butenyl)-1H-pyrrol-3-yl]phenylmethanone

: 863097-73-8
[4-(4-chloro-phenyl)-1-(3-methyl-but-2-enyl)-1H-pyrrol-3-yl]-phenyl-methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/jm048997u

Reference yield:

: 863097-41-0
[4-(4-chlorophenyl)-1-(3-methyl-2-butenyl)-1H-pyrrol-3-yl]phenylmethanone

: 1-{[4-(4-chloro-phenyl)-1-(3-methyl-but-2-enyl)-1H-pyrrol-3-yl]-phenyl-methyl}-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / 20 °C

2: 61 percent / acetonitrile / 48 h / 20 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm048997u