Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(BocNHC₆H₄)C₂₀H₈N₄C₄C₂₀H₈N₄(C₆H₄NHBoc)(C₆H₄(OCH₂CH₂)3OMe)2)

Base Information

• Chemical Name: Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(BocNHC₆H₄)C₂₀H₈N₄C₄C₂₀H₈N₄(C₆H₄NHBoc)(C₆H₄(OCH₂CH₂)3OMe)2)
• CAS No.: 1062503-79-0
• Molecular Formula: C₁₁₈H₁₂₀N₁₀O₂₀Zn₂
• Molecular Weight: 2129.09

Synonyms:Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(BocNHC₆H₄)C₂₀H₈N₄C₄C₂₀H₈N₄(C₆H₄NHBoc)(C₆H₄(OCH₂CH₂)3OMe)2)

Chemical Property of Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(BocNHC₆H₄)C₂₀H₈N₄C₄C₂₀H₈N₄(C₆H₄NHBoc)(C₆H₄(OCH₂CH₂)3OMe)2)

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Technology Process of Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(BocNHC₆H₄)C₂₀H₈N₄C₄C₂₀H₈N₄(C₆H₄NHBoc)(C₆H₄(OCH₂CH₂)3OMe)2)

There total 3 articles about Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(BocNHC₆H₄)C₂₀H₈N₄C₄C₂₀H₈N₄(C₆H₄NHBoc)(C₆H₄(OCH₂CH₂)3OMe)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C59H61N5O10Zn (1062503-78-9) → C118H120N10O20Zn2 (1062503-79-0)

Guidance literature:

C₅₉H₆₁N₅O₁₀Zn; With oxygen; In dichloromethane; for 0.25h;

With copper(l) chloride; In dichloromethane; for 0.0333333h;

With N,N,N,N,-tetramethylethylenediamine; In dichloromethane; for 1.5h;

Reference yield: 80.0%

Zn((3-MeO(CH2CH2O)3C6H4)2(BocHNC6H4)(HCC)C20H8N2) (1062503-78-9) → Zn2((MeO(CH2CH2O)3C6H4)2(BocNHC6H4)C20H8N4C4C20H8N4(C6H4NHBoc)(C6H4(OCH2CH2)3OMe)2) (1062503-79-0)

Guidance literature:

With air; copper(l) chloride; In dichloromethane; stirring CH2Cl2 soln. of porphyrin deriv. in air for 15 min, addn. of CuCl, stirring for 2 min, addn. of amine deriv., stirring for 90 min; addn. of water, washing with water, chromy. (silica, ethyl acetate/methanol (95:5)), evapn., NMR and MALDI;

DOI:10.1039/b814789b

Reference yield:

Zn((3-MeO(CH2CH2O)3C6H4)2(BocHNC6H4)(HCC)C20H8N2) (1062503-78-9) → C118H120N10O20Zn2 (1062503-79-0)

Guidance literature:

Zn((3-MeO(CH₂CH₂O)3C₆H₄)2(BocHNC₆H₄)(HCC)C₂₀H₈N₂); With copper(l) chloride; In dichloromethane; for 0.0333333h;

With N,N,N,N,-tetramethylethylenediamine; In dichloromethane; for 1.5h;

DOI:10.1039/b814789b

upstream raw materials:

C₅₉H₆₁N₅O₁₀Zn

Zn((3-MeO(CH₂CH₂O)3C₆H₄)2(BocHNC₆H₄)(HCC)C₂₀H₈N₂)

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