DL-4-(3,4-dimethyl-benzoyl-amino)-5-(di-n-pentylamino)-5-oxo-pentanoic acid methyl ester

Base Information

Chemical Name:DL-4-(3,4-dimethyl-benzoyl-amino)-5-(di-n-pentylamino)-5-oxo-pentanoic acid methyl ester
CAS No.:102743-20-4
Molecular Formula:C₂₅H₄₀N₂O₄
Molecular Weight:432.604
Hs Code.:

Synonyms:DL-4-(3,4-dimethyl-benzoyl-amino)-5-(di-n-pentylamino)-5-oxo-pentanoic acid methyl ester

Suppliers and Price of DL-4-(3,4-dimethyl-benzoyl-amino)-5-(di-n-pentylamino)-5-oxo-pentanoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of DL-4-(3,4-dimethyl-benzoyl-amino)-5-(di-n-pentylamino)-5-oxo-pentanoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of DL-4-(3,4-dimethyl-benzoyl-amino)-5-(di-n-pentylamino)-5-oxo-pentanoic acid methyl ester

There total 3 articles about DL-4-(3,4-dimethyl-benzoyl-amino)-5-(di-n-pentylamino)-5-oxo-pentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118710-00-2
DL-glutamic acid-γ-methyl ester hydrochloride

: 102743-20-4
DL-4-(3,4-dimethyl-benzoyl-amino)-5-(di-n-pentylamino)-5-oxo-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaHCO₃ / H₂O / 1.5 h / Ambient temperature

2: 1.) 1-hydroxybenzotriazol hydrate, N,N'-dicyclohexyl-carbodiimide / 1.) THF, 0.5 h, room temp., 2.) THF, room temp., overnight

With sodium hydrogencarbonate; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; In water;

Reference yield:

: 21900-23-2
3,4-dimethylbenzoyl chloride

: 102743-20-4
DL-4-(3,4-dimethyl-benzoyl-amino)-5-(di-n-pentylamino)-5-oxo-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaHCO₃ / H₂O / 1.5 h / Ambient temperature

2: 1.) 1-hydroxybenzotriazol hydrate, N,N'-dicyclohexyl-carbodiimide / 1.) THF, 0.5 h, room temp., 2.) THF, room temp., overnight

With sodium hydrogencarbonate; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; In water;

Reference yield:

: 102743-19-1
DL-N-(3,4-dimethyl-benzoyl)-glutamic acid-γ-methyl ester

: 2050-92-2
Di-n-amylamine

: 102743-20-4
DL-4-(3,4-dimethyl-benzoyl-amino)-5-(di-n-pentylamino)-5-oxo-pentanoic acid methyl ester

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; Multistep reaction; 1.) THF, 0.5 h, room temp., 2.) THF, room temp., overnight;