Sodium 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate

Base Information

• Chemical Name: Sodium 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate
• CAS No.: 89088-16-4
• Molecular Formula: C₂₇H₃₂N₃O₆*Na
• Molecular Weight: 517.557

Synonyms:Sodium 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate

Chemical Property of Sodium 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Sodium 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate

There total 4 articles about Sodium 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate (89088-15-3) → Sodium 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate (89088-16-4)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; at 25 ℃; for 1h;

DOI:10.1021/jo00180a011

Reference yield:

tyrosamine (51-67-2) → Sodium 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate (89088-16-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 98 percent / DIPEA / ethyl acetate / 20 h / 25 °C

2: 1. thallium ethoxide / 1. ether, 25 deg C, 2. a. DMF, 1h, 25 deg C, b. 20h, -15 deg C

3: 1.44 g / NaOH / tetrahydrofuran / 1 h / 25 °C

With sodium hydroxide; thallium (I) ethoxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethyl acetate;

DOI:10.1021/jo00180a011

Reference yield:

N-(tert-Butoxycarbonyl)-L-phenyl-alanyltyramide (89088-14-2) → Sodium 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate (89088-16-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1. thallium ethoxide / 1. ether, 25 deg C, 2. a. DMF, 1h, 25 deg C, b. 20h, -15 deg C

2: 1.44 g / NaOH / tetrahydrofuran / 1 h / 25 °C

With sodium hydroxide; thallium (I) ethoxide; In tetrahydrofuran;

DOI:10.1021/jo00180a011

upstream raw materials:

Methyl 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate

tyrosamine

N-(tert-Butoxycarbonyl)-L-phenyl-alanyltyramide

(tert-butoxycarbonyl)-L-phenylalanine N-hydroxysuccinimide ester

Downstream raw materials:

(5S,8R,9R)-5-Benzyl-1,2-dihydro-N^α-(N,N-dimethyl-L-alanyl-L-valyl)-N^α,9-ethylene-p-phencyclopeptine

Dihydromauritine A

(2R,3R)-3-{4-[2-((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-ethyl]-phenoxy}-1-[2-(2-dimethylamino-propionylamino)-3-methyl-butyryl]-pyrrolidine-2-carboxylic acid

(2S,3S)-3-{4-[2-((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-ethyl]-phenoxy}-1-[2-(2-dimethylamino-propionylamino)-3-methyl-butyryl]-pyrrolidine-2-carboxylic acid

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 89088-16-4 Sodium 3-amino>ethyl>phenoxy>-1-pyrroline-2-carboxylate

Send

Send

Metric Ton KG G Pound L ML

Send

Send