C₂₉H₃₆O₅Si

Base Information

Chemical Name:C₂₉H₃₆O₅Si
CAS No.:1394301-45-1
Molecular Formula:C₂₉H₃₆O₅Si
Molecular Weight:492.687
Hs Code.:

C<sub>29</sub>H<sub>36</sub>O<sub>5</sub>Si

Synonyms:C₂₉H₃₆O₅Si

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Chemical Property of C₂₉H₃₆O₅Si

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Technology Process of C₂₉H₃₆O₅Si

There total 5 articles about C₂₉H₃₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1394301-44-0
C₂₉H₃₄O₃Si

: 1394301-45-1
C₂₉H₃₆O₅Si

Guidance literature:: With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In acetone; at 0 - 20 ℃;
DOI:10.1021/ja305322x

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1394301-45-1
C₂₉H₃₆O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 20 °C

2.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; mineral oil / 12 h / 0 - 20 °C

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 4 h / 0 - 20 °C

4.1: acetic anhydride; dipyridinium dichromate / dichloromethane / 12 h / 20 °C

5.1: n-butyllithium / tetrahydrofuran / 0.67 h / -78 - 20 °C

5.2: 5 h / -78 - 0 °C

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide; water / acetone / 0 - 20 °C

With 1H-imidazole; triethylsilane; osmium(VIII) oxide; dipyridinium dichromate; n-butyllithium; boron trifluoride diethyl etherate; water; acetic anhydride; tetra-(n-butyl)ammonium iodide; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; mineral oil; 5.2: |Wittig Olefination;
DOI:10.1021/ja305322x

Reference yield:

: 114861-14-2
1,2-O-isopropylidene-5-O-(t-butyldiphenylsilyl)-α-D-xylofuranose

: 1394301-45-1
C₂₉H₃₆O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; mineral oil / 12 h / 0 - 20 °C

2.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 4 h / 0 - 20 °C

3.1: acetic anhydride; dipyridinium dichromate / dichloromethane / 12 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran / 0.67 h / -78 - 20 °C

4.2: 5 h / -78 - 0 °C

5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide; water / acetone / 0 - 20 °C

With triethylsilane; osmium(VIII) oxide; dipyridinium dichromate; n-butyllithium; boron trifluoride diethyl etherate; water; acetic anhydride; tetra-(n-butyl)ammonium iodide; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; mineral oil; 4.2: |Wittig Olefination;
DOI:10.1021/ja305322x