C₃₀H₃₇NO₃Si

Base Information

Chemical Name:C₃₀H₃₇NO₃Si
CAS No.:1312542-25-8
Molecular Formula:C₃₀H₃₇NO₃Si
Molecular Weight:487.714
Hs Code.:

C<sub>30</sub>H<sub>37</sub>NO<sub>3</sub>Si

Synonyms:C₃₀H₃₇NO₃Si

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Chemical Property of C₃₀H₃₇NO₃Si

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Technology Process of C₃₀H₃₇NO₃Si

There total 8 articles about C₃₀H₃₇NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1199940-92-5
C₁₄H₂₄O₃Si

: 1312542-25-8
C₃₀H₃₇NO₃Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: dichloromethane / 24 h / 25 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 0.5 h / -30 °C / Inrtert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 25 °C

4.1: N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide / tetrahydrofuran / 0.33 h / -20 °C

4.2: 0.5 h / -20 - 25 °C

5.1: hydrogenchloride / 72 h / 120 °C / Inert atmosphere; Molecular sieve

6.1: pyridine / 6 h / 25 °C

7.1: 2 h / 180 °C / vacuum

8.1: tetrahydrofuran / 0.5 h / -30 °C

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol201095b

Reference yield:

: 1312542-19-0
C₃₄H₄₉NO₆SSi₂

: 1312542-25-8
C₃₀H₃₇NO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide / tetrahydrofuran / 0.33 h / -20 °C

1.2: 0.5 h / -20 - 25 °C

2.1: hydrogenchloride / 72 h / 120 °C / Inert atmosphere; Molecular sieve

3.1: pyridine / 6 h / 25 °C

4.1: 2 h / 180 °C / vacuum

5.1: tetrahydrofuran / 0.5 h / -30 °C

With pyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; In tetrahydrofuran;
DOI:10.1021/ol201095b

Reference yield:

: 1312542-18-9
C₂₈H₃₅NO₆SSi

: 1312542-25-8
C₃₀H₃₇NO₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 25 °C

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide / tetrahydrofuran / 0.33 h / -20 °C

2.2: 0.5 h / -20 - 25 °C

3.1: hydrogenchloride / 72 h / 120 °C / Inert atmosphere; Molecular sieve

4.1: pyridine / 6 h / 25 °C

5.1: 2 h / 180 °C / vacuum

6.1: tetrahydrofuran / 0.5 h / -30 °C

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol201095b