1-[4,4-bis-(4-chloro-phenyl)-3-iodo-but-3-enyl]-4-butyl-1H-[1,2,3]triazole

Base Information

Chemical Name:1-[4,4-bis-(4-chloro-phenyl)-3-iodo-but-3-enyl]-4-butyl-1H-[1,2,3]triazole
CAS No.:908295-52-3
Molecular Formula:C₂₂H₂₂Cl₂IN₃
Molecular Weight:526.247
Hs Code.:

1-[4,4-bis-(4-chloro-phenyl)-3-iodo-but-3-enyl]-4-butyl-1<i>H</i>-[1,2,3]triazole

Synonyms:1-[4,4-bis-(4-chloro-phenyl)-3-iodo-but-3-enyl]-4-butyl-1H-[1,2,3]triazole

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Chemical Property of 1-[4,4-bis-(4-chloro-phenyl)-3-iodo-but-3-enyl]-4-butyl-1H-[1,2,3]triazole

Chemical Property:

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Technology Process of 1-[4,4-bis-(4-chloro-phenyl)-3-iodo-but-3-enyl]-4-butyl-1H-[1,2,3]triazole

There total 3 articles about 1-[4,4-bis-(4-chloro-phenyl)-3-iodo-but-3-enyl]-4-butyl-1H-[1,2,3]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₂Cl₂IN₃

: 693-02-7
hex-1-yne

: 908295-52-3
1-[4,4-bis-(4-chloro-phenyl)-3-iodo-but-3-enyl]-4-butyl-1H-[1,2,3]triazole

Guidance literature:: With sodium hydroxide; copper(II) sulfate; ascorbic acid; In ethanol; at 70 ℃; for 20h;
DOI:10.1055/s-2006-939708

Reference yield:

: 214116-83-3
di(4-chlorophenyl)methylenecyclopropane

: 908295-52-3
1-[4,4-bis-(4-chloro-phenyl)-3-iodo-but-3-enyl]-4-butyl-1H-[1,2,3]triazole

Guidance literature:: Multi-step reaction with 3 steps

1: CuI; I₂ / acetonitrile

2: NaN₃ / aq. ethanol / Heating

3: aq. NaOH; ascorbic acid; CuSO₄ / ethanol / 20 h / 70 °C

With sodium hydroxide; copper(l) iodide; sodium azide; iodine; copper(II) sulfate; ascorbic acid; In ethanol; acetonitrile;
DOI:10.1055/s-2006-939708

Reference yield:

: 698389-76-3
2,4-diiodo-1,1-bis(4-chlorophenyl)but-1-ene

: 908295-52-3
1-[4,4-bis-(4-chloro-phenyl)-3-iodo-but-3-enyl]-4-butyl-1H-[1,2,3]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: NaN₃ / aq. ethanol / Heating

2: aq. NaOH; ascorbic acid; CuSO₄ / ethanol / 20 h / 70 °C

With sodium hydroxide; sodium azide; copper(II) sulfate; ascorbic acid; In ethanol;
DOI:10.1055/s-2006-939708