methyl (E)-3-(4-ethylphenyl)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)acrylate

Base Information

Chemical Name:methyl (E)-3-(4-ethylphenyl)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)acrylate
CAS No.:1353088-29-5
Molecular Formula:C₂₀H₂₁NO₄
Molecular Weight:339.391
Hs Code.:

Synonyms:methyl (E)-3-(4-ethylphenyl)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)acrylate

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Chemical Property of methyl (E)-3-(4-ethylphenyl)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)acrylate

Chemical Property:

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Technology Process of methyl (E)-3-(4-ethylphenyl)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)acrylate

There total 2 articles about methyl (E)-3-(4-ethylphenyl)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: C₂₀H₂₀O₄

: 1353088-29-5
methyl (E)-3-(4-ethylphenyl)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)acrylate

Guidance literature:: With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; water; at 20 ℃; for 1.5h;
DOI:10.1055/s-0031-1289707

Reference yield:

: 213999-87-2
methyl (2Z)-2-(bromomethyl)-3-(4-ethylphenyl)prop-2-enoate

: 1353088-29-5
methyl (E)-3-(4-ethylphenyl)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 3 h / 20 °C

2: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 1.5 h / 20 °C

With hydroxylamine hydrochloride; potassium carbonate; sodium hydroxide; In ethanol; water; acetonitrile;
DOI:10.1055/s-0031-1289707

Reference yield: 74.0%

: 1353088-29-5
methyl (E)-3-(4-ethylphenyl)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)acrylate

: methyl 3-(4-ethylphenyl)-3H-chromeno[4,3-c]isoxazole-3a(4H)-carboxylate

Guidance literature:: methyl (E)-3-(4-ethylphenyl)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)acrylate; With N-chloro-succinimide; In tetrachloromethane; at 0 - 10 ℃; for 3h;

With triethylamine; In tetrachloromethane; at 20 ℃; for 2h;
DOI:10.1055/s-0031-1289707