C₃₀H₃₈FN₇O₄Si

Base Information

• Chemical Name: C₃₀H₃₈FN₇O₄Si
• CAS No.: 1431873-89-0
• Molecular Formula: C₃₀H₃₈FN₇O₄Si
• Molecular Weight: 607.76
• Mol file: 1431873-89-0.mol

Synonyms:C₃₀H₃₈FN₇O₄Si

Chemical Property of C₃₀H₃₈FN₇O₄Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₈FN₇O₄Si

There total 9 articles about C₃₀H₃₈FN₇O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

C18H29NO5SSi (1431873-86-7) + C19H17FN6O2 (1431873-03-8) → C30H38FN7O4Si (1431873-89-0) + C30H38FN7O4Si (1431873-88-9)

Guidance literature:

C₁₉H₁₇FN₆O₂; With sodium hydride; In N,N-dimethyl-formamide; at 5 ℃; for 0.25h; Inert atmosphere;

C₁₈H₂₉NO₅SSi; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

C7H4BrN3O (1431872-97-7) → C30H38FN7O4Si (1431873-89-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 100 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C

3.1: hydrogenchloride / 1,4-dioxane / 100 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 5 °C / Inert atmosphere

4.2: 20 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; sodium carbonate; N,N-dimethyl-formamide; trichlorophosphate; In 1,4-dioxane; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

C8H8ClN3O2 (1431872-96-6) → C30H38FN7O4Si (1431873-89-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: hydrogen bromide; acetic acid / 3 h / 40 - 50 °C

2.1: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 2 h / Inert atmosphere; Reflux

4.1: hydrogenchloride / 1,4-dioxane / 100 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 5 °C / Inert atmosphere

5.2: 20 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen bromide; sodium hydride; sodium carbonate; acetic acid; N,N-dimethyl-formamide; trichlorophosphate; In 1,4-dioxane; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

upstream raw materials:

C₇H₄BrN₃O

C₁₈H₂₉NO₅SSi

C₁₉H₁₇FN₆O₂

C₁₁H₉N₅O