bis(4-(2-(4-(bis(2-methoxyethyl)amino)phenyl)ethynyl)phenyl)ethanedione

Base Information

• Chemical Name: bis(4-(2-(4-(bis(2-methoxyethyl)amino)phenyl)ethynyl)phenyl)ethanedione
• CAS No.: 1060627-04-4
• Molecular Formula: C₄₂H₄₄N₂O₆
• Molecular Weight: 672.821
• Mol file: 1060627-04-4.mol

Synonyms:bis(4-(2-(4-(bis(2-methoxyethyl)amino)phenyl)ethynyl)phenyl)ethanedione

Chemical Property of bis(4-(2-(4-(bis(2-methoxyethyl)amino)phenyl)ethynyl)phenyl)ethanedione

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of bis(4-(2-(4-(bis(2-methoxyethyl)amino)phenyl)ethynyl)phenyl)ethanedione

There total 1 articles about bis(4-(2-(4-(bis(2-methoxyethyl)amino)phenyl)ethynyl)phenyl)ethanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

4-iodo-N,N-bis(2-methoxyethyl)benzeneamine (849358-29-8) + 1,2-bis(4-ethynylphenyl)ethane-1,2-dione (254886-83-4) → bis(4-(2-(4-(bis(2-methoxyethyl)amino)phenyl)ethynyl)phenyl)ethanedione (1060627-04-4)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/ja8039025

Reference yield: 97.0%

bis(4-(2-(4-(bis(2-methoxyethyl)amino)phenyl)ethynyl)phenyl)ethanedione (1060627-04-4) → methyl 4-(2-(4-(bis(2-methoxyethyl)amino)phenyl)ethynyl)benzoate (1060627-07-7)

Guidance literature:

With tetra-n-butylammonium cyanide; In methanol; dichloromethane; at 20 ℃; for 0.166667h;

DOI:10.1021/ja8039025

upstream raw materials:

4-iodo-N,N-bis(2-methoxyethyl)benzeneamine

1,2-bis(4-ethynylphenyl)ethane-1,2-dione

Downstream raw materials:

methyl 4-(2-(4-(bis(2-methoxyethyl)amino)phenyl)ethynyl)benzoate