(S)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethyl)propane-2-sulfinamide

Base Information

Chemical Name:(S)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethyl)propane-2-sulfinamide
CAS No.:1383677-37-9
Molecular Formula:C₂₀H₂₃N₃OS
Molecular Weight:353.488
Hs Code.:

Synonyms:(S)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethyl)propane-2-sulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethyl)propane-2-sulfinamide

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Technology Process of (S)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethyl)propane-2-sulfinamide

There total 3 articles about (S)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethyl)propane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383677-30-2
(S,E)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethylidene)propane-2-sulfinamide

: 1383677-37-9
(S)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethyl)propane-2-sulfinamide

Guidance literature:: (S,E)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethylidene)propane-2-sulfinamide; With sodium tetrahydroborate; In tetrahydrofuran; at 0 - 20 ℃;

With water; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 1380602-44-7
1-(2-phenyl-1,8-naphthyridin-3-yl)ethanone

: 1383677-37-9
(S)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethyl)propane-2-sulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / Inert atmosphere; Reflux

2.1: sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C

2.2: 20 °C

With titanium(IV) tetraethanolate; sodium tetrahydroborate; In tetrahydrofuran;

Reference yield:

: 7521-41-7
2-Aminonicotinaldehyde

: 1383677-37-9
(S)-2-methyl-N-(1-(2-phenyl-1,8-naphthyridin-3-yl)ethyl)propane-2-sulfinamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / ethanol / 90 °C

2.1: acetic anhydride; chromium(VI) oxide; sulfuric acid; acetic acid / 24 h / 30 °C / Cooling with ice

3.1: titanium(IV) tetraethanolate / tetrahydrofuran / Inert atmosphere; Reflux

4.1: sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C

4.2: 20 °C

With chromium(VI) oxide; titanium(IV) tetraethanolate; sodium tetrahydroborate; sulfuric acid; acetic anhydride; acetic acid; potassium hydroxide; In tetrahydrofuran; ethanol;