tris(2-hydroxy-3-methyl-5-nitro-benzyl)-methylammonium iodide

Base Information

Chemical Name:tris(2-hydroxy-3-methyl-5-nitro-benzyl)-methylammonium iodide
CAS No.:1423460-28-9
Molecular Formula:C₂₅H₃₀NO₃*I
Molecular Weight:519.423
Hs Code.:

Synonyms:tris(2-hydroxy-3-methyl-5-nitro-benzyl)-methylammonium iodide

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Chemical Property of tris(2-hydroxy-3-methyl-5-nitro-benzyl)-methylammonium iodide

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Technology Process of tris(2-hydroxy-3-methyl-5-nitro-benzyl)-methylammonium iodide

There total 5 articles about tris(2-hydroxy-3-methyl-5-nitro-benzyl)-methylammonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422032-18-5
C₂₈H₃₆NO₃⁽¹⁺⁾*I^(1-)

: 1423460-28-9
tris(2-hydroxy-3-methyl-5-nitro-benzyl)-methylammonium iodide

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃;
DOI:10.1002/adsc.201200243

Reference yield:

: 824-42-0
2-methoxy-3-methylbenzaldehyde

: 1423460-28-9
tris(2-hydroxy-3-methyl-5-nitro-benzyl)-methylammonium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

2: ammonium acetate; sodium tris(acetoxy)borohydride / tetrahydrofuran / 20 °C

3: neat (no solvent) / 70 - 80 °C

4: boron tribromide / dichloromethane / -78 - 20 °C

With ammonium acetate; boron tribromide; sodium tris(acetoxy)borohydride; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201200243

Reference yield:

: 67639-61-6
2-methoxy-3-methylanisaldehyde

: 1423460-28-9
tris(2-hydroxy-3-methyl-5-nitro-benzyl)-methylammonium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate; sodium tris(acetoxy)borohydride / tetrahydrofuran / 20 °C

2: neat (no solvent) / 70 - 80 °C

3: boron tribromide / dichloromethane / -78 - 20 °C

With ammonium acetate; boron tribromide; sodium tris(acetoxy)borohydride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/adsc.201200243