4-<4-<(4-acetyl-3-hydroxy-2-propylphenyl)methoxy>phenyl>-4-oxo-3-methylbutanenitrile

Base Information

Chemical Name:4-<4-<(4-acetyl-3-hydroxy-2-propylphenyl)methoxy>phenyl>-4-oxo-3-methylbutanenitrile
CAS No.:119348-73-1
Molecular Formula:C₂₃H₂₅NO₄
Molecular Weight:379.456
Hs Code.:

Synonyms:4-<4-<(4-acetyl-3-hydroxy-2-propylphenyl)methoxy>phenyl>-4-oxo-3-methylbutanenitrile

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Chemical Property of 4-<4-<(4-acetyl-3-hydroxy-2-propylphenyl)methoxy>phenyl>-4-oxo-3-methylbutanenitrile

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Technology Process of 4-<4-<(4-acetyl-3-hydroxy-2-propylphenyl)methoxy>phenyl>-4-oxo-3-methylbutanenitrile

There total 3 articles about 4-<4-<(4-acetyl-3-hydroxy-2-propylphenyl)methoxy>phenyl>-4-oxo-3-methylbutanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 135312-36-6
4-(4-Hydroxy-phenyl)-3-methyl-4-oxo-butyronitrile

: 97582-36-0
1-<4-(chloromethyl)-2-hydroxy-3-propylphenyl>ethanone

: 119348-73-1
4-<4-<(4-acetyl-3-hydroxy-2-propylphenyl)methoxy>phenyl>-4-oxo-3-methylbutanenitrile

Guidance literature:: With potassium tert-butylate; sodium iodide; In ethanol; for 30h; Ambient temperature;
DOI:10.1021/jm00113a014

Reference yield:

: 135312-35-5
4-(4-methoxyphenyl)-3-methyl-4-oxobutanenitrile

: 119348-73-1
4-<4-<(4-acetyl-3-hydroxy-2-propylphenyl)methoxy>phenyl>-4-oxo-3-methylbutanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / aluminum chloride / CH₂Cl₂ / 20 h / Heating

2: 76 percent / potassium t-butoxide, NaI / ethanol / 30 h / Ambient temperature

With aluminium trichloride; potassium tert-butylate; sodium iodide; In ethanol; dichloromethane;
DOI:10.1021/jm00113a014

Reference yield:

: 121-97-1
4-Methoxypropiophenone

: 119348-73-1
4-<4-<(4-acetyl-3-hydroxy-2-propylphenyl)methoxy>phenyl>-4-oxo-3-methylbutanenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / LDA / tetrahydrofuran; hexane / 16 h / -60 - 20 °C

2: 62 percent / aluminum chloride / CH₂Cl₂ / 20 h / Heating

3: 76 percent / potassium t-butoxide, NaI / ethanol / 30 h / Ambient temperature

With aluminium trichloride; potassium tert-butylate; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane;
DOI:10.1021/jm00113a014