C₅₅H₅₉NO₁₅

Base Information

Chemical Name:C₅₅H₅₉NO₁₅
CAS No.:153145-55-2
Molecular Formula:C₅₅H₅₉NO₁₅
Molecular Weight:974.071
Hs Code.:

C<sub>55</sub>H<sub>59</sub>NO<sub>15</sub>

Synonyms:C₅₅H₅₉NO₁₅

Suppliers and Price of C₅₅H₅₉NO₁₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₅H₅₉NO₁₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₅H₅₉NO₁₅

There total 26 articles about C₅₅H₅₉NO₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153145-54-1
C₆₁H₇₃NO₁₅Si

: 153145-55-2
C₅₅H₅₉NO₁₅

Guidance literature:: With pyridine; hydrogen fluoride; In acetonitrile; at 0 ℃; for 1h;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

: 153145-55-2
C₅₅H₅₉NO₁₅

Guidance literature:: Multi-step reaction with 23 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

11: 63 percent / Burgess' reagent

12: 100 percent / pyridine

13: 65 percent / OsO₄

14: DBU / toluene / 2 h / 105 °C

15: 75 percent / pyridine, DMAP / 24 h / 25 °C

16: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

17: tetrahydrofuran / 0.17 h / -78 °C

18: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

19: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

20: pyridine, DMAP / 20 h / 25 °C

21: 94 percent / TASF / tetrahydrofuran / 1 h / 25 °C

22: 1.) LHMDS / 1.) THF, 2.) THF, 0 deg C, 1 h

23: HF, pyridine / acetonitrile / 1 h / 0 °C

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; hydrogen fluoride; potassium tert-butylate; tris(dimethylamino)sulfonium trimethylsilyldifluoride; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 153145-56-3
C₃₃H₅₆O₈Si₂

: 153145-55-2
C₅₅H₅₉NO₁₅

Guidance literature:: Multi-step reaction with 22 steps

1: KMnO₄, KH₂PO₄

3: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

4: 100 percent / p-TsOH

5: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

6: acid

7: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

8: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

9: 95 percent / CH₂Cl₂ / 15 h / -45 °C

10: 63 percent / Burgess' reagent

11: 100 percent / pyridine

12: 65 percent / OsO₄

13: DBU / toluene / 2 h / 105 °C

14: 75 percent / pyridine, DMAP / 24 h / 25 °C

15: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

16: tetrahydrofuran / 0.17 h / -78 °C

17: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

18: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

19: pyridine, DMAP / 20 h / 25 °C

20: 94 percent / TASF / tetrahydrofuran / 1 h / 25 °C

21: 1.) LHMDS / 1.) THF, 2.) THF, 0 deg C, 1 h

22: HF, pyridine / acetonitrile / 1 h / 0 °C

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; hydrogen fluoride; potassium tert-butylate; tris(dimethylamino)sulfonium trimethylsilyldifluoride; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;