2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-thiolate

Base Information

• Chemical Name: 2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-thiolate
• CAS No.: 1190690-38-0
• Molecular Formula: C₂₃H₂₀N₂S₂
• Molecular Weight: 388.557
• Mol file: 1190690-38-0.mol

Synonyms:2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-thiolate

Chemical Property of 2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-thiolate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-thiolate

There total 4 articles about 2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-olate (173094-31-0) → 2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-thiolate (1190690-38-0)

Guidance literature:

With p-nitrophenyl isothiocyanate; In N,N-dimethyl-formamide; at 20 ℃; chemoselective reaction;

DOI:10.1021/jo900960a

Reference yield: 80.0%

phenyl isothiocyanate (103-72-0) + 2-(N-methylbenzylamino)-3-(4-nitrophenyl)-5-phenyl-1,3-thiazolium-4-olate (173094-33-2) → 2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-thiolate (1190690-38-0) + 2-(N-methylbenzylamino)-3-(4-nitrophenyl)-5-phenyl-1,3-thiazolium-4-thiolate (1190690-40-4)

Guidance literature:

In N,N-dimethyl-formamide; at 20 - 100 ℃; for 0.0833333h; chemoselective reaction; Microwave irradiation;

DOI:10.1021/jo900960a

Reference yield: 75.0%

p-nitrophenyl isothiocyanate (2131-61-5) + 2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-olate (173094-31-0) → 2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-thiolate (1190690-38-0) + 2-(N-methylbenzylamino)-3-(4-nitrophenyl)-5-phenyl-1,3-thiazolium-4-thiolate (1190690-40-4)

Guidance literature:

In N,N-dimethyl-formamide; at 100 ℃; chemoselective reaction;

DOI:10.1021/jo900960a

upstream raw materials:

phenyl isothiocyanate

2-(N-methylbenzylamino)-3-(4-nitrophenyl)-5-phenyl-1,3-thiazolium-4-olate

4-Methoxyphenyl isothiocyanate

2-(N-methylbenzylamino)-3,5-diphenyl-1,3-thiazolium-4-olate