N-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-yl)-N',N'-bis[2-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-ylamino)ethyl]ethane-1,2-diamine

Base Information

Chemical Name:N-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-yl)-N',N'-bis[2-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-ylamino)ethyl]ethane-1,2-diamine
CAS No.:443295-35-0
Molecular Formula:C₁₁₄H₁₆₂N₄
Molecular Weight:1588.57
Hs Code.:

Synonyms:N-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-yl)-N',N'-bis[2-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-ylamino)ethyl]ethane-1,2-diamine

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Chemical Property of N-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-yl)-N',N'-bis[2-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-ylamino)ethyl]ethane-1,2-diamine

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Technology Process of N-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-yl)-N',N'-bis[2-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-ylamino)ethyl]ethane-1,2-diamine

There total 1 articles about N-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-yl)-N',N'-bis[2-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-ylamino)ethyl]ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: (N(CH₂CH₂N(3,5-(2,4,6-(iPr)3C₆H₂)2C₆H₃))3)Mo(dinirogen)

: 585524-03-4
[2,6-lutidinium][tetrakis[3,5-bis(trifluoromethyl)phenyl]borate]

: 443295-35-0
N-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-yl)-N',N'-bis[2-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-ylamino)ethyl]ethane-1,2-diamine

: [Mo(NH₃)((3,5-(2,4,6-(isopropyl)C₆H₂)2C₆H₃NCH₂CH₂)3N)][B(3,5-(CF₃)2C₆H₃)4]

Guidance literature:: With cobaltocene; In benzene; 7 equiv. of B compd. and 8.2 equiv. of Cp2Co in benzene added to Mo complex; detd. by (1)H NMR spectra;
DOI:10.1021/ja020186x

Reference yield: 86.0%

: 443295-35-0
N-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-yl)-N',N'-bis[2-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-ylamino)ethyl]ethane-1,2-diamine

: 131063-11-1,16997-51-6,19559-06-9
Vanadium (III) chloride-(tris-tetrahydrofuran)

: [(3,5-(2,4,6-i-Pr₃C₆H₂)2C₆H₃NCH₂CH₂)3N]V(THF)

Guidance literature:: With (TMS)2NLi; In tetrahydrofuran; byproducts: LiCl; under N2 atm. V complex and ligand in THF were stirred for 1 h, (TMS)2NLi was added and stirred for 1 h; solvent was removed in vacuo at room temp., residue was taken up in pentane, filtered through Celite, concd. and cooled to -35°C, dried in vacuo at room temp.; elem. anal.;
DOI:10.1021/ic061554r

Reference yield: 67.0%

: 443295-35-0
N-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-yl)-N',N'-bis[2-(2,4,6,2'',4'',6''-hexaisopropyl-[1,1':3',1'']terphenyl-5'-ylamino)ethyl]ethane-1,2-diamine

: 146733-16-6
tetrachloro(1,2-dimethoxyethane-O,O')tungsten(IV)

: [((3,5-(2,4,6-i-Pr₃C₆H₂)2C₆H₃NC₂H₄)3N)WCl]

Guidance literature:: With (Me₃Si)2NLi; In benzene; byproducts: LiCl; (N2); Schlenk technique; mixt. of W complex and ligand in C6H6 was stirred for 2 h; solid (Me3Si)2NLi was added over 10 min; soln. was stirred for 2 h; evapd. (vac.); dried at 70°C overnight; extd. (C6H6); filtered (Celite); concd.; centrifuged; evapd. (vac.); heated (85°C, severalh); triturated (C5H12); kept at -35°C overnight; filtered; washe d (C5H12); dried (vac.); elem. anal.;
DOI:10.1139/v05-013