N-{chloro[4-(4-propylcyclohexyl)phenyl]methylene}-N-methylmethanaminium chloride

Base Information

Chemical Name:N-{chloro[4-(4-propylcyclohexyl)phenyl]methylene}-N-methylmethanaminium chloride
CAS No.:1455481-75-0
Molecular Formula:C₁₈H₂₇ClN*Cl
Molecular Weight:328.325
Hs Code.:

Synonyms:N-{chloro[4-(4-propylcyclohexyl)phenyl]methylene}-N-methylmethanaminium chloride

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Chemical Property of N-{chloro[4-(4-propylcyclohexyl)phenyl]methylene}-N-methylmethanaminium chloride

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Technology Process of N-{chloro[4-(4-propylcyclohexyl)phenyl]methylene}-N-methylmethanaminium chloride

There total 3 articles about N-{chloro[4-(4-propylcyclohexyl)phenyl]methylene}-N-methylmethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1455481-69-2
C₁₈H₂₇NO

: 1455481-75-0
N-{chloro[4-(4-propylcyclohexyl)phenyl]methylene}-N-methylmethanaminium chloride

Guidance literature:: With oxalyl dichloride; In toluene; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2013.07.062

Reference yield:

: trans-4-(4-n-propylcyclohexyl)benzoic acid

: 1455481-75-0
N-{chloro[4-(4-propylcyclohexyl)phenyl]methylene}-N-methylmethanaminium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / Inert atmosphere; Reflux

2: Inert atmosphere

3: oxalyl dichloride / toluene / 12 h / 80 °C / Inert atmosphere

With thionyl chloride; oxalyl dichloride; In toluene;
DOI:10.1016/j.tet.2013.07.062

Reference yield:

: 82492-58-8
4-(trans-4'-propylcyclohexyl) benzoic acid chloride

: 1455481-75-0
N-{chloro[4-(4-propylcyclohexyl)phenyl]methylene}-N-methylmethanaminium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: Inert atmosphere

2: oxalyl dichloride / toluene / 12 h / 80 °C / Inert atmosphere

With oxalyl dichloride; In toluene;
DOI:10.1016/j.tet.2013.07.062