C₅₄H₅₆O₈Si₂

Base Information

Chemical Name:C₅₄H₅₆O₈Si₂
CAS No.:1352916-62-1
Molecular Formula:C₅₄H₅₆O₈Si₂
Molecular Weight:889.205
Hs Code.:

C<sub>54</sub>H<sub>56</sub>O<sub>8</sub>Si<sub>2</sub>

Synonyms:C₅₄H₅₆O₈Si₂

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Chemical Property of C₅₄H₅₆O₈Si₂

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Technology Process of C₅₄H₅₆O₈Si₂

There total 10 articles about C₅₄H₅₆O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1352916-61-0
C₂₂H₂₀O₈

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1352916-62-1
C₅₄H₅₆O₈Si₂

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1002/anie.201104504

Reference yield:

: 1352916-43-8
C₃₀H₄₀O₉Si

: 1352916-62-1
C₅₄H₅₆O₈Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium triethylborohydride / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.1: dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

3.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 15 h / 0 °C / Inert atmosphere

4.1: pyridine; Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.1: sodium chlorite; disodium hydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 0 °C / Inert atmosphere

6.1: trifluoroacetic anhydride / nitromethane / 2.5 h / 80 °C / Inert atmosphere; Molecular sieve

6.2: 2 h / 20 °C / Inert atmosphere

7.1: 1H-imidazole; dmap / dichloromethane / 20 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; sodium chlorite; disodium hydrogenphosphate; 2-methyl-but-2-ene; lithium triethylborohydride; Dess-Martin periodane; pyridine hydrogenfluoride; trifluoroacetic anhydride; In tetrahydrofuran; nitromethane; dichloromethane; water; tert-butyl alcohol; 6.1: Friedel Crafts acylation;
DOI:10.1002/anie.201104504

Reference yield:

: 1352916-53-0
C₃₅H₅₀O₁₁Si

: 1352916-62-1
C₅₄H₅₆O₈Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 15 h / 0 °C / Inert atmosphere

2.1: pyridine; Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.1: sodium chlorite; disodium hydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 0 °C / Inert atmosphere

4.1: trifluoroacetic anhydride / nitromethane / 2.5 h / 80 °C / Inert atmosphere; Molecular sieve

4.2: 2 h / 20 °C / Inert atmosphere

5.1: 1H-imidazole; dmap / dichloromethane / 20 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; sodium chlorite; disodium hydrogenphosphate; 2-methyl-but-2-ene; Dess-Martin periodane; pyridine hydrogenfluoride; trifluoroacetic anhydride; In tetrahydrofuran; nitromethane; dichloromethane; water; tert-butyl alcohol; 4.1: Friedel Crafts acylation;
DOI:10.1002/anie.201104504