NIH 10772

Base Information

• Chemical Name: NIH 10772
• CAS No.: 160625-35-4
• Molecular Formula: C₂₁H₂₄N₂O₃
• Molecular Weight: 352.433

Synonyms:NIH 10772

Chemical Property of NIH 10772

Chemical Property:

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Technology Process of NIH 10772

There total 2 articles about NIH 10772 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+)-cis-N-Normetazocine (16670-83-0) → NIH 10772 (160625-35-4)

Guidance literature:

With sodium hydrogencarbonate; In ethanol; for 4h; Heating;

DOI:10.1021/jm00003a019

Reference yield:

(+)-cis-N-Normetazocine (16670-83-0) + 1-bromomethyl-4-nitro-benzene (100-11-8) → NIH 10772 (160625-35-4)

Guidance literature:

With sodium hydrogencarbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jm010501a

Reference yield:

NIH 10772 (160625-35-4) → (+)-(2S,6S,11S)-3-(4-aminobenzyl)-6,11-dimethyl-1,2,3,4,5,6-hexahydro-2,6-methano-3-benzazocin-8-ol (160625-40-1)

Guidance literature:

With hydrogenchloride; nickel boride; In ethanol; at 50 ℃; for 5h;

DOI:10.1021/jm00003a019

upstream raw materials:

(+)-cis-N-Normetazocine

1-bromomethyl-4-nitro-benzene

Downstream raw materials:

(+)-(2S,6S,11S)-3-(4-aminobenzyl)-6,11-dimethyl-1,2,3,4,5,6-hexahydro-2,6-methano-3-benzazocin-8-ol

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