(E)-3-[(dimethylphenylsilyl)methyl]-4-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene]-1-tosylpyrrolidine

Base Information

Chemical Name:(E)-3-[(dimethylphenylsilyl)methyl]-4-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene]-1-tosylpyrrolidine
CAS No.:1260620-16-3
Molecular Formula:C₂₇H₃₈BNO₄SSi
Molecular Weight:511.566
Hs Code.:

Synonyms:(E)-3-[(dimethylphenylsilyl)methyl]-4-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene]-1-tosylpyrrolidine

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Chemical Property of (E)-3-[(dimethylphenylsilyl)methyl]-4-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene]-1-tosylpyrrolidine

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Technology Process of (E)-3-[(dimethylphenylsilyl)methyl]-4-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene]-1-tosylpyrrolidine

There total 1 articles about (E)-3-[(dimethylphenylsilyl)methyl]-4-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene]-1-tosylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: C₁₄H₁₆O₂S

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 1260620-16-3
(E)-3-[(dimethylphenylsilyl)methyl]-4-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene]-1-tosylpyrrolidine

Guidance literature:: With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride; methylmagnesium chloride; In tetrahydrofuran; at -35 - 50 ℃; for 25h; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201000434

Reference yield: 88.0%

: 106-39-8
bromochlorobenzene

: 1260620-16-3
(E)-3-[(dimethylphenylsilyl)methyl]-4-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene]-1-tosylpyrrolidine

: 1260620-50-5
(E)-3-(4-chlorobenzylidene)-4-[(dimethylphenylsilyl)-methyl]-1-tosylpyrrolidine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; at 80 ℃; for 18h; Inert atmosphere;
DOI:10.1002/adsc.201000434

Reference yield: 87.0%

: 108-86-1,52753-63-6
bromobenzene

: 1260620-16-3
(E)-3-[(dimethylphenylsilyl)methyl]-4-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene]-1-tosylpyrrolidine

: 1260620-26-5
(E)-3-benzylidene-4-[(dimethylphenylsilyl)methyl]-1-tosylpyrrolidine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; at 80 ℃; for 18h; Inert atmosphere;
DOI:10.1002/adsc.201000434