p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside
CAS No.:1393114-52-7
Molecular Formula:C₄₈H₄₅NO₁₃
Molecular Weight:843.884
Hs Code.:

Synonyms:p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

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Chemical Property of p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

There total 1 articles about p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1187765-97-4
ethyl 2-O-benzoyl-3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside

: 138906-43-1
4-methoxyphenyl 4,6-di-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 1393114-52-7
p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

: C₄₈H₄₅NO₁₃

Guidance literature:: ethyl 2-O-benzoyl-3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside; 4-methoxyphenyl 4,6-di-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -30 - 0 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1007/s10719-012-9383-4

Reference yield: 68.0%

: 1393114-52-7
p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

: 1393114-58-3
(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->3)-(4,6-di-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α/β-D-galactopyranosyl trichloroacetimidate

: p-methoxyphenyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->3)-(4,6-di-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-galactopyranosyl)-(1->3)-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

: C₉₉H₁₀₄N₄O₃₃

Guidance literature:: With perchloric acid supported over silica; In diethyl ether; dichloromethane; at -10 ℃; for 1h;
DOI:10.1007/s10719-012-9383-4