(C₄H₂SC₂H)2C₁₀H₄

Base Information

Chemical Name:(C₄H₂SC₂H)2C₁₀H₄
CAS No.:335157-75-0
Molecular Formula:C₂₂H₁₀S₂
Molecular Weight:338.453
Hs Code.:

(C<sub>4</sub>H<sub>2</sub>SC<sub>2</sub>H)2C<sub>10</sub>H<sub>4</sub>

Synonyms:(C₄H₂SC₂H)2C₁₀H₄

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Chemical Property of (C₄H₂SC₂H)2C₁₀H₄

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Technology Process of (C₄H₂SC₂H)2C₁₀H₄

There total 3 articles about (C₄H₂SC₂H)2C₁₀H₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 335157-68-1
(C₄H₂SC₂SiC₃H₉)2C₁₀H₄

: 335157-75-0
(C₄H₂SC₂H)2C₁₀H₄

Guidance literature:: With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃;
DOI:10.1021/ol015511k

Reference yield:

: 335157-64-7
(C₄H₂SBr)2C₁₀H₄

: 335157-75-0
(C₄H₂SC₂H)2C₁₀H₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / diethyl ether / 0.75 h / -78 °C

1.2: 90 percent / I₂ / diethyl ether / -78 - 0 °C

2.1: 86 percent / PdCl₂(PPh₃)2; CuI; NH(i-Pr)2 / toluene / 70 °C

3.1: 84 percent / K₂CO₃ / methanol; tetrahydrofuran / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; potassium carbonate; diisopropylamine; In tetrahydrofuran; methanol; diethyl ether; toluene; 2.1: Sonogashira coupling;
DOI:10.1021/ol015511k

Reference yield:

: 335157-65-8
(C₄H₂SI)2C₁₀H₄

: 335157-75-0
(C₄H₂SC₂H)2C₁₀H₄

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / PdCl₂(PPh₃)2; CuI; NH(i-Pr)2 / toluene / 70 °C

2: 84 percent / K₂CO₃ / methanol; tetrahydrofuran / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; diisopropylamine; In tetrahydrofuran; methanol; toluene; 1: Sonogashira coupling;
DOI:10.1021/ol015511k