methyl 4-<2-(3-benzyloxyphenyl)-2-hydroxyethylaminocarbonylmethyl>cinnamate

Base Information

Chemical Name:methyl 4-<2-(3-benzyloxyphenyl)-2-hydroxyethylaminocarbonylmethyl>cinnamate
CAS No.:154349-05-0
Molecular Formula:C₂₇H₂₇NO₅
Molecular Weight:445.515
Hs Code.:

Synonyms:methyl 4-<2-(3-benzyloxyphenyl)-2-hydroxyethylaminocarbonylmethyl>cinnamate

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Chemical Property of methyl 4-<2-(3-benzyloxyphenyl)-2-hydroxyethylaminocarbonylmethyl>cinnamate

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Technology Process of methyl 4-<2-(3-benzyloxyphenyl)-2-hydroxyethylaminocarbonylmethyl>cinnamate

There total 3 articles about methyl 4-<2-(3-benzyloxyphenyl)-2-hydroxyethylaminocarbonylmethyl>cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 62932-74-5
2-amino-1-[3-(benzyloxy)phenyl]ethan-1-ol

: 154349-04-9
(E)-4-(2-methoxycarbonylvinyl)phenylacetyl chloride

: 154349-05-0
methyl 4-<2-(3-benzyloxyphenyl)-2-hydroxyethylaminocarbonylmethyl>cinnamate

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; diethyl ether; for 1.5h;
DOI:10.1002/jhet.5570300622

Reference yield:

: 154349-03-8
(E)-2-[4-(3-methoxy-3-oxoprop-1-en-1-yl)phenyl]acetic acid

: 154349-05-0
methyl 4-<2-(3-benzyloxyphenyl)-2-hydroxyethylaminocarbonylmethyl>cinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / SOCl₂ / benzene / 1.5 h / Heating

2: 80 percent / 1N NaOH / dioxane; diethyl ether / 1.5 h

With sodium hydroxide; thionyl chloride; In 1,4-dioxane; diethyl ether; benzene;
DOI:10.1002/jhet.5570300622

Reference yield:

: 1878-68-8
2-(4-bromophenyl)-acetic acid

: 154349-05-0
methyl 4-<2-(3-benzyloxyphenyl)-2-hydroxyethylaminocarbonylmethyl>cinnamate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / triphenylphosphine, palladium acetate, diisopropylethylamine / 72 h / 100 °C

2: 100 percent / SOCl₂ / benzene / 1.5 h / Heating

3: 80 percent / 1N NaOH / dioxane; diethyl ether / 1.5 h

With sodium hydroxide; thionyl chloride; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In 1,4-dioxane; diethyl ether; benzene;
DOI:10.1002/jhet.5570300622