Technology Process of tert-butyl (S)-1-(((perylen-3-yl)methoxy)carbonyl)-2-phenylethylcarbamate
There total 3 articles about tert-butyl (S)-1-(((perylen-3-yl)methoxy)carbonyl)-2-phenylethylcarbamate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / tetrahydrofuran
2: phosphorus tribromide / tetrachloromethane / 4 h / 80 °C
3: hydrogen fluoride; potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C
With
sodium tetrahydroborate; hydrogen fluoride; phosphorus tribromide; potassium carbonate;
In
tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.11.074
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trichlorophosphate / 1,2-dichloro-benzene
2: sodium tetrahydroborate / tetrahydrofuran
3: phosphorus tribromide / tetrachloromethane / 4 h / 80 °C
4: hydrogen fluoride; potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C
With
sodium tetrahydroborate; hydrogen fluoride; phosphorus tribromide; potassium carbonate; trichlorophosphate;
In
tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide; 1,2-dichloro-benzene;
DOI:10.1016/j.tet.2011.11.074
- Guidance literature:
-
Multi-step reaction with 2 steps
1: phosphorus tribromide / tetrachloromethane / 4 h / 80 °C
2: hydrogen fluoride; potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C
With
hydrogen fluoride; phosphorus tribromide; potassium carbonate;
In
tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.11.074