Technology Process of 3-((4-(benzyloxy)-3-bromo-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid
There total 2 articles about 3-((4-(benzyloxy)-3-bromo-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1-(benzyloxy)-2,4-dibromoanthracene-9,10-dione; meta-aminobenzoic acid;
With
potassium acetate; copper diacetate; copper;
In
pentan-1-ol;
at 150 - 160 ℃;
for 20h;
With
hydrogenchloride; water;
at 80 - 90 ℃;
for 0.166667h;
DOI:10.1016/j.bmc.2012.06.002
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / N,N-dimethyl-formamide; butanone / 20 h / Reflux
2.1: potassium acetate; copper diacetate; copper / pentan-1-ol / 20 h / 150 - 160 °C
2.2: 0.17 h / 80 - 90 °C
With
potassium acetate; copper diacetate; copper; potassium carbonate;
In
pentan-1-ol; N,N-dimethyl-formamide; butanone;
DOI:10.1016/j.bmc.2012.06.002
