Technology Process of C38H41FN4O11S
There total 8 articles about C38H41FN4O11S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N,N,N,N,N,N-hexamethylphosphoric triamide;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ja310659j
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium hydroxide; Tris(3,6-dioxaheptyl)amine / toluene / 20 °C
2: dmap / tetrahydrofuran / 20 °C / Sealed tube
3: hydrogenchloride / tetrahydrofuran; water / 20 °C
4: pyridine / 20 °C
5: tetra-(n-butyl)ammonium iodide; sodium hydroxide / toluene; water
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C
7: N,N,N,N,N,N-hexamethylphosphoric triamide / 20 °C / Inert atmosphere
With
pyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; Tris(3,6-dioxaheptyl)amine; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; water; toluene;
DOI:10.1021/ja310659j
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium hydroxide; Tris(3,6-dioxaheptyl)amine / toluene / 20 °C
2: dmap / tetrahydrofuran / 20 °C / Sealed tube
3: hydrogenchloride / tetrahydrofuran; water / 20 °C
4: pyridine / 20 °C
5: tetra-(n-butyl)ammonium iodide; sodium hydroxide / toluene; water
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C
7: N,N,N,N,N,N-hexamethylphosphoric triamide / 20 °C / Inert atmosphere
With
pyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; Tris(3,6-dioxaheptyl)amine; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; water; toluene;
DOI:10.1021/ja310659j