tert-butyl (1R,2Z,4S,5R,6R,7R)-N-benzyl-5,6,7-tris(benzyloxy)-4-hydroxycyclohept-2-enylcarbamate

Base Information

Chemical Name:tert-butyl (1R,2Z,4S,5R,6R,7R)-N-benzyl-5,6,7-tris(benzyloxy)-4-hydroxycyclohept-2-enylcarbamate
CAS No.:1236156-24-3
Molecular Formula:C₄₀H₄₅NO₆
Molecular Weight:635.8
Hs Code.:

Synonyms:tert-butyl (1R,2Z,4S,5R,6R,7R)-N-benzyl-5,6,7-tris(benzyloxy)-4-hydroxycyclohept-2-enylcarbamate

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Chemical Property of tert-butyl (1R,2Z,4S,5R,6R,7R)-N-benzyl-5,6,7-tris(benzyloxy)-4-hydroxycyclohept-2-enylcarbamate

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Technology Process of tert-butyl (1R,2Z,4S,5R,6R,7R)-N-benzyl-5,6,7-tris(benzyloxy)-4-hydroxycyclohept-2-enylcarbamate

There total 2 articles about tert-butyl (1R,2Z,4S,5R,6R,7R)-N-benzyl-5,6,7-tris(benzyloxy)-4-hydroxycyclohept-2-enylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1236156-22-1
C₄₀H₄₃NO₆

: 1236156-24-3
tert-butyl (1R,2Z,4S,5R,6R,7R)-N-benzyl-5,6,7-tris(benzyloxy)-4-hydroxycyclohept-2-enylcarbamate

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride heptahydrate; In methanol; at 20 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1002/ejoc.201000157

Reference yield: 37.0%

: 1236156-19-6
tert-butyl (1E,3R,4R,5R,6R,7S)-N-benzyl-4,5,6-tris(benzyloxy)-7-hydroxy-1-phenylnona-1,8-dien-3-ylcarbamate

: 1236156-24-3
tert-butyl (1R,2Z,4S,5R,6R,7R)-N-benzyl-5,6,7-tris(benzyloxy)-4-hydroxycyclohept-2-enylcarbamate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 90 ℃; for 6h; under 5171.62 Torr; Inert atmosphere; Microwave irradiation;
DOI:10.1002/ejoc.201000157