1-benzyl-4-azepanone oxime

Base Information

Chemical Name:1-benzyl-4-azepanone oxime
CAS No.:82102-84-9
Molecular Formula:C₁₃H₁₈N₂O
Molecular Weight:218.299
Hs Code.:

Synonyms:1-benzyl-4-azepanone oxime

Suppliers and Price of 1-benzyl-4-azepanone oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-4-azepanone oxime

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 1-benzyl-4-azepanone oxime

There total 1 articles about 1-benzyl-4-azepanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1208-75-9
1-benzylazepan-4-one

: 82102-84-9
1-benzyl-4-azepanone oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; for 1.5h; Reflux;
DOI:10.1016/j.bmcl.2012.01.045

Reference yield: 37.0%

: 82102-84-9
1-benzyl-4-azepanone oxime

: 109105-51-3
1-benzyl-hexahydro-azepin-4-ylamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 24h; Inert atmosphere; Reflux;
DOI:10.1016/j.bmcl.2012.01.045

Reference yield:

: 82102-84-9
1-benzyl-4-azepanone oxime

: 1365212-48-1
C₁₅H₂₀N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere; Reflux

2: triethylamine / chloroform / 20 °C / Inert atmosphere

3: palladium on activated charcoal; hydrogen / ethanol / 3361.55 Torr / Inert atmosphere

4: triethylamine / chloroform / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; palladium on activated charcoal; hydrogen; triethylamine; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1016/j.bmcl.2012.01.045