8-(methoxycarbonyl)octyl 3,6-bis-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-α-D-mannopyranoside

Base Information

Chemical Name:8-(methoxycarbonyl)octyl 3,6-bis-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-α-D-mannopyranoside
CAS No.:108167-24-4
Molecular Formula:C₁₃₂H₁₄₈O₄₀P₂
Molecular Weight:2436.55
Hs Code.:

8-(methoxycarbonyl)octyl 3,6-bis-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-α-D-mannopyranoside

Synonyms:8-(methoxycarbonyl)octyl 3,6-bis-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-α-D-mannopyranoside

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Chemical Property of 8-(methoxycarbonyl)octyl 3,6-bis-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-α-D-mannopyranoside

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Technology Process of 8-(methoxycarbonyl)octyl 3,6-bis-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-α-D-mannopyranoside

There total 2 articles about 8-(methoxycarbonyl)octyl 3,6-bis-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 108167-22-2
8-(methoxycarbonyl)octyl 2,4-di-O-benzyl-3,6-bis-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

: 108266-23-5
2,3,4-tri-O-acetyl-6-O-<(diphenoxy)phosphoryl>-α-D-mannopyranosyl bromide

: 108167-24-4
8-(methoxycarbonyl)octyl 3,6-bis-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-α-D-mannopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In 1,2-dichloro-ethane; for 144h; Ambient temperature;
DOI:10.1021/jo00389a039

Reference yield:

: 108167-22-2
8-(methoxycarbonyl)octyl 2,4-di-O-benzyl-3,6-bis-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

: 108266-23-5
2,3,4-tri-O-acetyl-6-O-<(diphenoxy)phosphoryl>-α-D-mannopyranosyl bromide

: 108167-27-7
8-(methoxycarbonyl)octyl 3-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-6-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

: 108167-26-6
8-(methoxycarbonyl)octyl 6-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-3-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

: 108167-24-4
8-(methoxycarbonyl)octyl 3,6-bis-O-<2-O-<2,3,4-tri-O-acetyl-6-O-(diphenylphosphoryl)-α-D-mannopyranosyl>-3,4,6-tri-O-benzyl-α-D-mannopyranosyl>-2,4-di-O-benzyl-α-D-mannopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In 1,2-dichloro-ethane; for 144h; Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo00389a039