3-<2-(E-carboethoxymethylidene)-1-phenylhydrazonoglyoxal-1-yl>-2(1H)-quinoxalinone

Base Information

Chemical Name:3-<2-(E-carboethoxymethylidene)-1-phenylhydrazonoglyoxal-1-yl>-2(1H)-quinoxalinone
CAS No.:113314-06-0
Molecular Formula:C₂₀H₁₈N₄O₃
Molecular Weight:362.388
Hs Code.:

Synonyms:3-<2-(E-carboethoxymethylidene)-1-phenylhydrazonoglyoxal-1-yl>-2(1H)-quinoxalinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<2-(E-carboethoxymethylidene)-1-phenylhydrazonoglyoxal-1-yl>-2(1H)-quinoxalinone

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Technology Process of 3-<2-(E-carboethoxymethylidene)-1-phenylhydrazonoglyoxal-1-yl>-2(1H)-quinoxalinone

There total 5 articles about 3-<2-(E-carboethoxymethylidene)-1-phenylhydrazonoglyoxal-1-yl>-2(1H)-quinoxalinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 68636-57-7
3-[1-(phenylhydrazono)glyoxal-1-yl]-2-quinoxalinone

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 113314-06-0
3-<2-(E-carboethoxymethylidene)-1-phenylhydrazonoglyoxal-1-yl>-2(1H)-quinoxalinone

Guidance literature:: In N,N-dimethyl-formamide; at 100 ℃; for 4h;

Reference yield: 73.0%

: 68636-57-7
(3-Oxo-3,4-dihydro-quinoxalin-2-yl)-(phenyl-hydrazono)-acetaldehyde

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 113314-09-3
3-<1-phenyl-6(1H)-pyridazinon-3-yl>-2(1H)-quinoxalinone

: 113314-06-0
(E)-4-(3-Oxo-3,4-dihydro-quinoxalin-2-yl)-4-(phenyl-hydrazono)-but-2-enoic acid ethyl ester

Guidance literature:: DOI:10.1016/S0008-6215(00)85220-9

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 113314-06-0
3-<2-(E-carboethoxymethylidene)-1-phenylhydrazonoglyoxal-1-yl>-2(1H)-quinoxalinone

Guidance literature:: Multi-step reaction with 4 steps

3: NaIO₄

4: 76 percent / dimethylformamide / 4 h / 100 °C

With sodium periodate; In N,N-dimethyl-formamide;