N-(4-cyanophenyl)-1,1,1-trifluoro-N-((trifluoromethyl)sulfonyl)methanesulfonamide

Base Information

• Chemical Name: N-(4-cyanophenyl)-1,1,1-trifluoro-N-((trifluoromethyl)sulfonyl)methanesulfonamide
• CAS No.: 1415694-01-7
• Molecular Formula: C₉H₄F₆N₂O₄S₂
• Molecular Weight: 382.264

Synonyms:N-(4-cyanophenyl)-1,1,1-trifluoro-N-((trifluoromethyl)sulfonyl)methanesulfonamide

Chemical Property of N-(4-cyanophenyl)-1,1,1-trifluoro-N-((trifluoromethyl)sulfonyl)methanesulfonamide

Chemical Property:

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Technology Process of N-(4-cyanophenyl)-1,1,1-trifluoro-N-((trifluoromethyl)sulfonyl)methanesulfonamide

There total 1 articles about N-(4-cyanophenyl)-1,1,1-trifluoro-N-((trifluoromethyl)sulfonyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

trifluoromethylsulfonic anhydride (358-23-6) + 4-Aminobenzonitrile (873-74-5) → N-(4-cyanophenyl)-1,1,1-trifluoro-N-((trifluoromethyl)sulfonyl)methanesulfonamide (1415694-01-7)

Guidance literature:

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c8cc00938d

Reference yield: 92.0%

4-Phenylpyridine 1-oxide (1131-61-9) + N-(4-cyanophenyl)-1,1,1-trifluoro-N-((trifluoromethyl)sulfonyl)methanesulfonamide (1415694-01-7) → 4-phenylpyridin-2-yl trifluoromethanesulfonate (392658-04-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/jo302014c

Reference yield: 66.0%

4-Phenylpyridine 1-oxide (1131-61-9) + N-(4-cyanophenyl)-1,1,1-trifluoro-N-((trifluoromethyl)sulfonyl)methanesulfonamide (1415694-01-7) → N-(4-cyanophenyl)-1,1,1-trifluoro-N-(4-phenylpyridin-2-yl)-methanesulfonamide (1415693-99-0) + 4-phenylpyridin-2-yl trifluoromethanesulfonate (392658-04-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In neat liquid; at 60 ℃; for 0.25h; Inert atmosphere;

DOI:10.1021/jo302014c

upstream raw materials:

trifluoromethylsulfonic anhydride

4-Aminobenzonitrile

Downstream raw materials:

N-(4-cyanophenyl)-1,1,1-trifluoro-N-(4-phenylpyridin-2-yl)-methanesulfonamide

4-phenylpyridin-2-yl trifluoromethanesulfonate

1,4-dimethoxy-2-(trifluoromethyl)benzene

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