benzyl 2,6,6'-tri-O-benzyl-3,2'-O-(3,6,9-trioxaundecane-1,11-diyl)-β-lactoside

Base Information

Chemical Name:benzyl 2,6,6'-tri-O-benzyl-3,2'-O-(3,6,9-trioxaundecane-1,11-diyl)-β-lactoside
CAS No.:105165-59-1
Molecular Formula:C₄₈H₆₀O₁₄
Molecular Weight:860.996
Hs Code.:

Synonyms:benzyl 2,6,6'-tri-O-benzyl-3,2'-O-(3,6,9-trioxaundecane-1,11-diyl)-β-lactoside

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Chemical Property of benzyl 2,6,6'-tri-O-benzyl-3,2'-O-(3,6,9-trioxaundecane-1,11-diyl)-β-lactoside

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Technology Process of benzyl 2,6,6'-tri-O-benzyl-3,2'-O-(3,6,9-trioxaundecane-1,11-diyl)-β-lactoside

There total 3 articles about benzyl 2,6,6'-tri-O-benzyl-3,2'-O-(3,6,9-trioxaundecane-1,11-diyl)-β-lactoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 105165-58-0
benzyl 2,6,6'-tri-O-benzyl-3',4'-O-isopropylidene-3,2'-O-(3,6,9.trioxaundecane-1,11-diyl)-β-lactoside

: 105165-59-1
benzyl 2,6,6'-tri-O-benzyl-3,2'-O-(3,6,9-trioxaundecane-1,11-diyl)-β-lactoside

Guidance literature:: With acetic acid; In ethanol; at 75 ℃; for 48h;
DOI:10.1016/0008-6215(86)80008-8

Reference yield:

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 105165-59-1
benzyl 2,6,6'-tri-O-benzyl-3,2'-O-(3,6,9-trioxaundecane-1,11-diyl)-β-lactoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium hydroxide / 1.) tetrahydrofuran, 45 deg C, 15 m, 2.) tetrahydrofuran, 65 deg C

2: 85 percent / aqueous 70percent acetic acid / ethanol / 48 h / 75 °C

With potassium hydroxide; acetic acid; In ethanol;
DOI:10.1016/0008-6215(86)80008-8

Reference yield:

: 105186-56-9
benzyl 2,6,6'-tri-O-benzyl-3',4'-O-isopropylidene-β-lactoside

: 105165-59-1
benzyl 2,6,6'-tri-O-benzyl-3,2'-O-(3,6,9-trioxaundecane-1,11-diyl)-β-lactoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium hydroxide / 1.) tetrahydrofuran, 45 deg C, 15 m, 2.) tetrahydrofuran, 65 deg C

2: 85 percent / aqueous 70percent acetic acid / ethanol / 48 h / 75 °C

With potassium hydroxide; acetic acid; In ethanol;
DOI:10.1016/0008-6215(86)80008-8