2-(tert-butyl-diphenyl-silanyloxymethyl)-7-aza-bicyclo[2.2.1]heptane-7-carboxylic acid tert-butyl ester

Base Information

Chemical Name:2-(tert-butyl-diphenyl-silanyloxymethyl)-7-aza-bicyclo[2.2.1]heptane-7-carboxylic acid tert-butyl ester
CAS No.:455330-46-8
Molecular Formula:C₂₈H₃₉NO₃Si
Molecular Weight:465.708
Hs Code.:

2-(<i>tert</i>-butyl-diphenyl-silanyloxymethyl)-7-aza-bicyclo[2.2.1]heptane-7-carboxylic acid <i>tert</i>-butyl ester

Synonyms:2-(tert-butyl-diphenyl-silanyloxymethyl)-7-aza-bicyclo[2.2.1]heptane-7-carboxylic acid tert-butyl ester

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Chemical Property of 2-(tert-butyl-diphenyl-silanyloxymethyl)-7-aza-bicyclo[2.2.1]heptane-7-carboxylic acid tert-butyl ester

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Technology Process of 2-(tert-butyl-diphenyl-silanyloxymethyl)-7-aza-bicyclo[2.2.1]heptane-7-carboxylic acid tert-butyl ester

There total 10 articles about 2-(tert-butyl-diphenyl-silanyloxymethyl)-7-aza-bicyclo[2.2.1]heptane-7-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 455330-55-9
methanesulfonic acid 4-tert-butoxycarbonylamino-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohexyl ester

: 455330-46-8
2-(tert-butyl-diphenyl-silanyloxymethyl)-7-aza-bicyclo[2.2.1]heptane-7-carboxylic acid tert-butyl ester

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide; benzene;

Reference yield:

: 96894-00-7
(1S,2S)-4,4-ethylenedioxy-2-hydroxymethylcyclohexanol

: 455330-46-8
2-(tert-butyl-diphenyl-silanyloxymethyl)-7-aza-bicyclo[2.2.1]heptane-7-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 84 percent / imidazole; DMAP / dimethylformamide

2: 100 percent / aq. acetic acid / dimethylformamide

3: 92 percent / DMAP / pyridine

4: 86 percent / sodium borohydride / methanol

5: 95 percent / sodium azide / dimethylformamide

6: 90 percent / DMAP / pyridine

7: 98 percent / hydrogen / Pd/C / methanol

8: 71 percent / potassium tert-butoxide / dimethylformamide; benzene

With 1H-imidazole; dmap; sodium tetrahydroborate; sodium azide; potassium tert-butylate; hydrogen; acetic acid; palladium on activated charcoal; In pyridine; methanol; N,N-dimethyl-formamide; benzene;

Reference yield:

: 96893-99-1
(1R,2S)-5,5-(Ethylendioxy)-2-hydroxycyclohexancarbonsaeure-ethylester

: 455330-46-8
2-(tert-butyl-diphenyl-silanyloxymethyl)-7-aza-bicyclo[2.2.1]heptane-7-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 10 steps

1: 98 percent / DMAP / pyridine

2: 99 percent / lithium aluminum hydride / diethyl ether

3: 84 percent / imidazole; DMAP / dimethylformamide

4: 100 percent / aq. acetic acid / dimethylformamide

5: 92 percent / DMAP / pyridine

6: 86 percent / sodium borohydride / methanol

7: 95 percent / sodium azide / dimethylformamide

8: 90 percent / DMAP / pyridine

9: 98 percent / hydrogen / Pd/C / methanol

10: 71 percent / potassium tert-butoxide / dimethylformamide; benzene

With 1H-imidazole; dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; sodium azide; potassium tert-butylate; hydrogen; acetic acid; palladium on activated charcoal; In pyridine; methanol; diethyl ether; N,N-dimethyl-formamide; benzene;