Technology Process of 5,6,7-tri-O-benzyl-2,3,4,8-tetradeoxy-4,8-imino-D-altro-octono-1,4-lactam
There total 15 articles about 5,6,7-tri-O-benzyl-2,3,4,8-tetradeoxy-4,8-imino-D-altro-octono-1,4-lactam which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 76 percent / 20percent acetic acid / H2O / 1 h / 80 °C
2: 63 percent / pyridine
3: 91 percent / H2 / 10percent Pd/C / ethanol / 2327.2 Torr
4: 4.7 g / sodium acetate / ethanol / Heating
5: sodium bicarbonate / ethanol; H2O / 2 h
6: 77 percent / hydrochloric acid / CHCl3 / 9 h
7: 79 percent / sodium hydride / dimethylformamide / 2 h
8: 93 percent / mercuric chloride, cadmium carbonate / acetone; H2O / 1 h / Heating
9: 82 percent / acetonitrile / 16 h / Heating
10: 1.) H2; 2.) sodium acetate / 1.) 10percent Pd/C / 1.) ethanol, 18 h; 2.) boiling, 20 h
With
hydrogenchloride; cadmium(II) carbonate; hydrogen; sodium acetate; sodium hydride; sodium hydrogencarbonate; acetic acid; mercury dichloride;
palladium on activated charcoal;
In
pyridine; ethanol; chloroform; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/S0040-4020(01)89805-7
- Guidance literature:
-
With
hydrogen; sodium acetate;
palladium on activated charcoal;
Yield given. Multistep reaction;
1.) ethanol, 18 h; 2.) boiling, 20 h;
DOI:10.1016/S0040-4020(01)89805-7
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 4.7 g / sodium acetate / ethanol / Heating
2: sodium bicarbonate / ethanol; H2O / 2 h
3: 77 percent / hydrochloric acid / CHCl3 / 9 h
4: 79 percent / sodium hydride / dimethylformamide / 2 h
5: 93 percent / mercuric chloride, cadmium carbonate / acetone; H2O / 1 h / Heating
6: 82 percent / acetonitrile / 16 h / Heating
7: 1.) H2; 2.) sodium acetate / 1.) 10percent Pd/C / 1.) ethanol, 18 h; 2.) boiling, 20 h
With
hydrogenchloride; cadmium(II) carbonate; hydrogen; sodium acetate; sodium hydride; sodium hydrogencarbonate; mercury dichloride;
palladium on activated charcoal;
In
ethanol; chloroform; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/S0040-4020(01)89805-7
