Technology Process of C37H50O6
There total 6 articles about C37H50O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
5-methylhex-1-yne;
With
sec.-butyllithium;
In
tetrahydrofuran;
at -78 ℃;
C30H38O6;
In
tetrahydrofuran;
DOI:10.1016/S0960-894X(02)00937-X
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 90 percent / iPr2NEt; Bu4NI / tetrahydrofuran
2.1: 94 percent / ppts; (MeO)3CH / methanol
3.1: 100 percent / DMSO; (COCl)2; Et3N / CH2Cl2 / -78 - 20 °C
4.1: s-BuLi / tetrahydrofuran / -78 °C
4.2: 86 percent / tetrahydrofuran
With
oxalyl dichloride; sec.-butyllithium; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; trimethyl orthoformate;
In
tetrahydrofuran; methanol; dichloromethane;
3.1: Swern oxidation;
DOI:10.1016/S0960-894X(02)00937-X
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 90 percent / iPr2NEt; Bu4NI / tetrahydrofuran
2.1: 94 percent / ppts; (MeO)3CH / methanol
3.1: 100 percent / DMSO; (COCl)2; Et3N / CH2Cl2 / -78 - 20 °C
4.1: s-BuLi / tetrahydrofuran / -78 °C
4.2: 86 percent / tetrahydrofuran
With
oxalyl dichloride; sec.-butyllithium; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; trimethyl orthoformate;
In
tetrahydrofuran; methanol; dichloromethane;
3.1: Swern oxidation;
DOI:10.1016/S0960-894X(02)00937-X
