dimethyl 2-{[(1-{[(benzyloxy)carbonyl]amino}-2-methylpropyl)(methoxy)phosphoryl]methyl}pentanedioate

Base Information

Chemical Name:dimethyl 2-{[(1-{[(benzyloxy)carbonyl]amino}-2-methylpropyl)(methoxy)phosphoryl]methyl}pentanedioate
CAS No.:939403-21-1
Molecular Formula:C₂₁H₃₂NO₈P
Molecular Weight:457.461
Hs Code.:

Synonyms:dimethyl 2-{[(1-{[(benzyloxy)carbonyl]amino}-2-methylpropyl)(methoxy)phosphoryl]methyl}pentanedioate

Suppliers and Price of dimethyl 2-{[(1-{[(benzyloxy)carbonyl]amino}-2-methylpropyl)(methoxy)phosphoryl]methyl}pentanedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl 2-{[(1-{[(benzyloxy)carbonyl]amino}-2-methylpropyl)(methoxy)phosphoryl]methyl}pentanedioate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of dimethyl 2-{[(1-{[(benzyloxy)carbonyl]amino}-2-methylpropyl)(methoxy)phosphoryl]methyl}pentanedioate

There total 2 articles about dimethyl 2-{[(1-{[(benzyloxy)carbonyl]amino}-2-methylpropyl)(methoxy)phosphoryl]methyl}pentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.2%

: 939403-19-7
methyl 1-{[(benzyloxy)carbonyl]amino}-2-methylpropylphosphinate

: 14035-94-0
dimethyl 2-methylglutarate

: 939403-21-1
dimethyl 2-{[(1-{[(benzyloxy)carbonyl]amino}-2-methylpropyl)(methoxy)phosphoryl]methyl}pentanedioate

Guidance literature:: With sodium methylate; In methanol; at 20 ℃;
DOI:10.1002/ardp.200600191

Reference yield:

: 65577-59-5
<1-<<(phenylmethoxy)carbonyl>amino>-2-methylpropyl>phosphinic acid

: 939403-21-1
dimethyl 2-{[(1-{[(benzyloxy)carbonyl]amino}-2-methylpropyl)(methoxy)phosphoryl]methyl}pentanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: EDC / 12 h

2: 39.2 percent / NaOMe / methanol / 20 °C

With sodium methylate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In methanol;
DOI:10.1002/ardp.200600191

Reference yield:

: 939403-21-1
dimethyl 2-{[(1-{[(benzyloxy)carbonyl]amino}-2-methylpropyl)(methoxy)phosphoryl]methyl}pentanedioate

: 939403-25-5
dimethyl 2-{[methoxy(2-methyl-1-{[(4-nitrobenzyl)sulfonyl]amino}propyl)phosphoryl]methyl}pentanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol / 1292.9 Torr

2: Et₃N / CH₂Cl₂ / 0 - 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1002/ardp.200600191