Technology Process of 4-Methoxy-5-methyl-2-nitrobenzamide
There total 6 articles about 4-Methoxy-5-methyl-2-nitrobenzamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sulfuric acid; water;
at 100 - 110 ℃;
for 2.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ethanol; water; potassium carbonate / 1 h / Heating / reflux
2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C
3: 1-methyl-pyrrolidin-2-one / 20 h / 140 - 150 °C
4: sulfuric acid; water / 2.5 h / 100 - 110 °C
With
ethanol; sulfuric acid; water; potassium carbonate;
In
1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / 1,1-dichloroethane; water; acetone / 3 h / Heating / reflux
2: sulfuric acid; nitric acid / 1 h / 5 - 10 °C
3: ethanol; water; potassium carbonate / 1 h / Heating / reflux
4: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C
5: 1-methyl-pyrrolidin-2-one / 20 h / 140 - 150 °C
6: sulfuric acid; water / 2.5 h / 100 - 110 °C
With
sodium hydroxide; ethanol; sulfuric acid; water; nitric acid; potassium carbonate;
In
1-methyl-pyrrolidin-2-one; 1,1-dichloroethane; water; N,N-dimethyl-formamide; acetone;
