4,4',4''-[(benzyloxy)methanetriyl]tris(1-benzyl-1H-1,2,3-triazole)*CuCl

Base Information

Chemical Name:4,4',4''-[(benzyloxy)methanetriyl]tris(1-benzyl-1H-1,2,3-triazole)*CuCl
CAS No.:1262106-01-3
Molecular Formula:C₃₅H₃₁ClCuN₉O
Molecular Weight:692.69
Hs Code.:

Synonyms:4,4',4''-[(benzyloxy)methanetriyl]tris(1-benzyl-1H-1,2,3-triazole)*CuCl

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Chemical Property of 4,4',4''-[(benzyloxy)methanetriyl]tris(1-benzyl-1H-1,2,3-triazole)*CuCl

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Technology Process of 4,4',4''-[(benzyloxy)methanetriyl]tris(1-benzyl-1H-1,2,3-triazole)*CuCl

There total 6 articles about 4,4',4''-[(benzyloxy)methanetriyl]tris(1-benzyl-1H-1,2,3-triazole)*CuCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1262106-00-2
4,4',4''-[(benzyloxy)methanetriyl]tris(1-benzyl-1H-1,2,3-triazole)

: copper(l) chloride

: 1262106-01-3
4,4',4''-[(benzyloxy)methanetriyl]tris(1-benzyl-1H-1,2,3-triazole)*CuCl

Guidance literature:: In 1,4-dioxane; at 60 ℃; for 6h;

Reference yield:

: 118569-20-3
1,5-bis(trimethylsilyl)-3-(2-(trimethylsilyl)ethynyl)penta-1,4-diyn-3-ol

: 1262106-01-3
4,4',4''-[(benzyloxy)methanetriyl]tris(1-benzyl-1H-1,2,3-triazole)*CuCl

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; methanol / 4 h / 20 °C

1.2: 6 h

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / -20 - 20 °C / Inert atmosphere

2.2: 14 h / 0 - 20 °C / Inert atmosphere

3.1: 1,4-dioxane / 6 h / 60 °C

With methanol; sodium hydride; potassium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 622-79-7
benzyl azide

: 1262106-01-3
4,4',4''-[(benzyloxy)methanetriyl]tris(1-benzyl-1H-1,2,3-triazole)*CuCl

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; methanol / 4 h / 20 °C

1.2: 6 h

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / -20 - 20 °C / Inert atmosphere

2.2: 14 h / 0 - 20 °C / Inert atmosphere

3.1: 1,4-dioxane / 6 h / 60 °C

With methanol; sodium hydride; potassium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide; mineral oil;