2-(3,4-DICHLORO-PHENYL)-SUCCINIC ACID

Base Information

• Chemical Name: 2-(3,4-DICHLORO-PHENYL)-SUCCINIC ACID
• CAS No.: 93553-81-2
• Molecular Formula: C10H8 Cl2 O4
• Molecular Weight: 263.07
• Hs Code.: 2917399090
• Mol file: 93553-81-2.mol

Synonyms:Butanedioicacid, (3,4-dichlorophenyl)- (9CI); Succinic acid, (3,4-dichlorophenyl)- (6CI)

Chemical Property of 2-(3,4-DICHLORO-PHENYL)-SUCCINIC ACID

Chemical Property:

• Vapor Pressure: 3.7E-06mmHg at 25°C
• Boiling Point: 370.9°C at 760 mmHg
• Flash Point: 178.1°C
• PSA: 74.60000
• Density: 1.555g/cm³
• LogP: 2.63630
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-(3,4-Dichlorophenyl)succinicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(3,4-DICHLORO-PHENYL)-SUCCINIC ACID

There total 4 articles about 2-(3,4-DICHLORO-PHENYL)-SUCCINIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.8%

3,4-dichlorophenyl-α,β-dicyanoethyl propionate (1412409-44-9) → 3,4-dichlorophenylsuccinic acid (93553-81-2)

Guidance literature:

With hydrogenchloride; In water; Reflux;

DOI:10.2174/157340612802084234

Reference yield:

ethyl 2-cyano-3-(3,4-dichlorophenyl)-prop-2-enecarboxylate (55417-50-0) → 3,4-dichlorophenylsuccinic acid (93553-81-2)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / water / 1.5 h / Reflux

2: hydrogenchloride / water / Reflux

With hydrogenchloride; ethanol; In water;

DOI:10.2174/157340612802084234

Reference yield:

3,4-dichlorobenzaldehyde (6287-38-3) → 3,4-dichlorophenylsuccinic acid (93553-81-2)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine; acetic acid / benzene / 20 h / Reflux

2: ethanol / water / 1.5 h / Reflux

3: hydrogenchloride / water / Reflux

With pyridine; hydrogenchloride; ethanol; acetic acid; In water; benzene;

DOI:10.2174/157340612802084234

upstream raw materials:

3,4-dichlorobenzaldehyde

ethyl 2-cyano-3-(3,4-dichlorophenyl)-prop-2-enecarboxylate

3,4-dichlorophenyl-α,β-dicyanoethyl propionate

Downstream raw materials:

1-Amino-3-(3,4-dichloro-phenyl)-pyrrolidine-2,5-dione

4-[3-(3,4-Dichloro-phenyl)-2,5-dioxo-pyrrolidin-1-yl]-benzenesulfonamide

5,6-dichloroindan-1-carboxylic acid

3-(3,4-dichlorophenyl)succinimide