α-chloro-N-[4-(5H-pyrrolo[2,1-c][1,4]benzodiazepin-10(11H)-ylcarbonyl)phenyl]benzeneacetamide

Base Information

Chemical Name:α-chloro-N-[4-(5H-pyrrolo[2,1-c][1,4]benzodiazepin-10(11H)-ylcarbonyl)phenyl]benzeneacetamide
CAS No.:168079-66-1
Molecular Formula:C₂₇H₂₂ClN₃O₂
Molecular Weight:455.944
Hs Code.:

Synonyms:α-chloro-N-[4-(5H-pyrrolo[2,1-c][1,4]benzodiazepin-10(11H)-ylcarbonyl)phenyl]benzeneacetamide

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Chemical Property of α-chloro-N-[4-(5H-pyrrolo[2,1-c][1,4]benzodiazepin-10(11H)-ylcarbonyl)phenyl]benzeneacetamide

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Technology Process of α-chloro-N-[4-(5H-pyrrolo[2,1-c][1,4]benzodiazepin-10(11H)-ylcarbonyl)phenyl]benzeneacetamide

There total 7 articles about α-chloro-N-[4-(5H-pyrrolo[2,1-c][1,4]benzodiazepin-10(11H)-ylcarbonyl)phenyl]benzeneacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2912-62-1
α-chlorophenylacetyl chloride

: 168078-59-9
10,11-dihydro-10-(4-aminobenzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

: 168079-66-1
α-chloro-N-[4-(5H-pyrrolo[2,1-c][1,4]benzodiazepin-10(11H)-ylcarbonyl)phenyl]benzeneacetamide

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield:

: 168078-58-8
10,11-dihydro-10(4-nitrobenzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

: 168079-66-1
α-chloro-N-[4-(5H-pyrrolo[2,1-c][1,4]benzodiazepin-10(11H)-ylcarbonyl)phenyl]benzeneacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / palladium-carbon / ethanol

2: triethylamine / dichloromethane

With triethylamine; hydrazine; palladium-carbon; In ethanol; dichloromethane;

Reference yield:

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 168079-66-1
α-chloro-N-[4-(5H-pyrrolo[2,1-c][1,4]benzodiazepin-10(11H)-ylcarbonyl)phenyl]benzeneacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / 2-pyrrole aldehyde; N,N-dimethyl-formamide; mineral oil

2: hydrogen / palladium-carbon / ethanol; ethyl acetate

3: triethylamine / dichloromethane

4: hydrazine / palladium-carbon / ethanol

5: triethylamine / dichloromethane

With sodium hydride; hydrogen; triethylamine; hydrazine; palladium-carbon; In 2-pyrrole aldehyde; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;