2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbohydrazide

Base Information

Chemical Name:2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbohydrazide
CAS No.:1620951-83-8
Molecular Formula:C₂₃H₂₁N₅O₂
Molecular Weight:399.452
Hs Code.:

Synonyms:2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbohydrazide

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Chemical Property of 2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbohydrazide

Chemical Property:

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Technology Process of 2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbohydrazide

There total 8 articles about 2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620955-23-8
C₂₄H₂₁N₃O₃

: 1620951-83-8
2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbohydrazide

Guidance literature:: With hydrazine hydrate; at 90 ℃; for 5h;

Reference yield:

: 191338-94-0
ethyl {4-[(2,2-dimethylpropanoyl)amino]pyridin-3-yl}(oxo)acetate

: 1620951-83-8
2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide; water / ethanol / 2 h / Reflux

1.2: 16 h

2.1: methanol; diethyl ether / 1 h / 0 °C

3.1: potassium carbonate / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere

3.2: 5 h / 80 °C

4.1: hydrazine hydrate / 5 h / 90 °C

With water; potassium carbonate; hydrazine hydrate; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; water;

Reference yield:

: 1054478-77-1
2-(4-bromophenyl)-1,6-naphthyridine-4-carboxylic acid

: 1620951-83-8
2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; diethyl ether / 1 h / 0 °C

2.1: potassium carbonate / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere

2.2: 5 h / 80 °C

3.1: hydrazine hydrate / 5 h / 90 °C

With potassium carbonate; hydrazine hydrate; In tetrahydrofuran; methanol; diethyl ether; water;