4-[allyl-(3,5-bis-trifluoromethyl-benzyl)-carbamoyl]-pent-4-enoic acid methyl ester

Base Information

Chemical Name:4-[allyl-(3,5-bis-trifluoromethyl-benzyl)-carbamoyl]-pent-4-enoic acid methyl ester
CAS No.:1415410-96-6
Molecular Formula:C₁₉H₁₉F₆NO₃
Molecular Weight:423.355
Hs Code.:

Synonyms:4-[allyl-(3,5-bis-trifluoromethyl-benzyl)-carbamoyl]-pent-4-enoic acid methyl ester

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Chemical Property of 4-[allyl-(3,5-bis-trifluoromethyl-benzyl)-carbamoyl]-pent-4-enoic acid methyl ester

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Technology Process of 4-[allyl-(3,5-bis-trifluoromethyl-benzyl)-carbamoyl]-pent-4-enoic acid methyl ester

There total 1 articles about 4-[allyl-(3,5-bis-trifluoromethyl-benzyl)-carbamoyl]-pent-4-enoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5621-44-3
dimethyl 2-methylenepentanedioate

: 1415410-96-6
4-[allyl-(3,5-bis-trifluoromethyl-benzyl)-carbamoyl]-pent-4-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: camphor-10-sulfonic acid / methanol / 2.5 h / 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

With dmap; camphor-10-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1002/cmdc.201300393

Reference yield: 98.0%

: 1415410-96-6
4-[allyl-(3,5-bis-trifluoromethyl-benzyl)-carbamoyl]-pent-4-enoic acid methyl ester

: 1415411-27-6
3-[1-(3,5-bis-trifluoromethyl-benzyl)-2-oxo-2,5-dihydro-1H-pyrrol-3-yl]-propionic acid methyl ester

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 12h; Inert atmosphere; Reflux; Darkness;
DOI:10.1021/jm3009376

Reference yield:

: 1415410-96-6
4-[allyl-(3,5-bis-trifluoromethyl-benzyl)-carbamoyl]-pent-4-enoic acid methyl ester

: 1415411-53-8
C₁₆H₁₄F₆N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / Inert atmosphere; Reflux; Darkness

2: hydroxylamine potassium salt / methanol / 12 h / 0 - 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydroxylamine potassium salt; In methanol; dichloromethane;
DOI:10.1021/jm3009376