p-methoxyphenylacetic acid 2-(methoxycarbonyl)phenyl ester

Base Information

Chemical Name:p-methoxyphenylacetic acid 2-(methoxycarbonyl)phenyl ester
CAS No.:1276694-79-1
Molecular Formula:C₁₇H₁₆O₅
Molecular Weight:300.311
Hs Code.:

Synonyms:p-methoxyphenylacetic acid 2-(methoxycarbonyl)phenyl ester

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Chemical Property of p-methoxyphenylacetic acid 2-(methoxycarbonyl)phenyl ester

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Technology Process of p-methoxyphenylacetic acid 2-(methoxycarbonyl)phenyl ester

There total 1 articles about p-methoxyphenylacetic acid 2-(methoxycarbonyl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 104-01-8
4-Methoxyphenylacetic acid

: 119-36-8,8024-54-2
methyl salicylate

: 1276694-79-1
p-methoxyphenylacetic acid 2-(methoxycarbonyl)phenyl ester

Guidance literature:: With pyridine; trichlorophosphate; at 0 - 10 ℃; for 3.5h;

Reference yield: 78.0%

: 1276694-79-1
p-methoxyphenylacetic acid 2-(methoxycarbonyl)phenyl ester

: 26151-95-1
4-hydroxy-3-(4-methoxyphenyl)-2H-chromen-2-one

Guidance literature:: With caesium carbonate; In acetone; at 20 ℃; for 7.5h; Time; Reagent/catalyst; Solvent;
DOI:10.1248/cpb.c13-00604

Reference yield:

: 1276694-79-1
p-methoxyphenylacetic acid 2-(methoxycarbonyl)phenyl ester

: 3-(4-methoxyphenyl)-4-(4-methylphenylamino)-2H-chromen-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide; pyridine / 5 h / 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 20 °C

2.2: 0.67 h / 20 °C / Cooling with ice

3.1: caesium carbonate / ethanol / 2 h / 75 °C

With pyridine; caesium carbonate; triethylamine; potassium hydroxide; In ethanol; dichloromethane;