Technology Process of C31H34N2O7
There total 7 articles about C31H34N2O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C31H37BN2O9;
With
dmap;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Molecular sieve;
With
copper diacetate;
In
dichloromethane;
at 20 ℃;
for 48h;
Molecular sieve;
DOI:10.1002/chem.201103185
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / dimethyl sulfoxide / 20 h / 80 °C / Inert atmosphere
2.1: sodium periodate; ammonium acetate; water / acetone / 17 h / 20 °C
3.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 1 h / 0 °C
3.2: 1 h / 20 °C
4.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 1 h / 0 °C
4.2: 24 h / 20 °C
5.1: dmap / dichloromethane / 0.5 h / 20 °C / Molecular sieve
5.2: 48 h / 20 °C / Molecular sieve
With
dmap; sodium periodate; 1-hydroxy-7-aza-benzotriazole; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; lithium hydroxide monohydrate; ammonium acetate; water; potassium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; chloroform; dimethyl sulfoxide; acetone;
DOI:10.1002/chem.201103185
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium periodate; ammonium acetate; water / acetone / 17 h / 20 °C
2.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 1 h / 0 °C
2.2: 1 h / 20 °C
3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 1 h / 0 °C
3.2: 24 h / 20 °C
4.1: dmap / dichloromethane / 0.5 h / 20 °C / Molecular sieve
4.2: 48 h / 20 °C / Molecular sieve
With
dmap; sodium periodate; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; ammonium acetate; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; chloroform; acetone;
DOI:10.1002/chem.201103185
