methyl (2S,5R)-2-(4-allyloxybenzyl)-3-aza-5-(9H-9-fluorenylmethyloxycarbonylamino)-8-guanidino-4-oxooctanoate hydrochloride

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Chemical Name:methyl (2S,5R)-2-(4-allyloxybenzyl)-3-aza-5-(9H-9-fluorenylmethyloxycarbonylamino)-8-guanidino-4-oxooctanoate hydrochloride
CAS No.:900521-46-2
Molecular Formula:C₃₄H₃₉N₅O₆*ClH
Molecular Weight:650.174
Hs Code.:

Synonyms:methyl (2S,5R)-2-(4-allyloxybenzyl)-3-aza-5-(9H-9-fluorenylmethyloxycarbonylamino)-8-guanidino-4-oxooctanoate hydrochloride

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Chemical Property of methyl (2S,5R)-2-(4-allyloxybenzyl)-3-aza-5-(9H-9-fluorenylmethyloxycarbonylamino)-8-guanidino-4-oxooctanoate hydrochloride

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Technology Process of methyl (2S,5R)-2-(4-allyloxybenzyl)-3-aza-5-(9H-9-fluorenylmethyloxycarbonylamino)-8-guanidino-4-oxooctanoate hydrochloride

There total 2 articles about methyl (2S,5R)-2-(4-allyloxybenzyl)-3-aza-5-(9H-9-fluorenylmethyloxycarbonylamino)-8-guanidino-4-oxooctanoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 900521-38-2
methyl (2S,5R)-2-(4-allyloxybenzyl)-3-aza-5-(9H-9-fluorenylmethyloxycarbonylamino)-4-oxo-8-[N'-(2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl)guanidino]octanoate

: 900521-46-2
methyl (2S,5R)-2-(4-allyloxybenzyl)-3-aza-5-(9H-9-fluorenylmethyloxycarbonylamino)-8-guanidino-4-oxooctanoate hydrochloride

Guidance literature:: methyl (2S,5R)-2-(4-allyloxybenzyl)-3-aza-5-(9H-9-fluorenylmethyloxycarbonylamino)-4-oxo-8-[N'-(2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl)guanidino]octanoate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;

With hydrogenchloride; In methanol; diethyl ether; water;
DOI:10.1016/j.tet.2008.09.031