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C9H8N2O2S

Base Information
  • Chemical Name:C9H8N2O2S
  • CAS No.:1093121-35-7
  • Molecular Formula:C9H8N2O2S
  • Molecular Weight:208.241
  • Hs Code.:
C<sub>9</sub>H<sub>8</sub>N<sub>2</sub>O<sub>2</sub>S

Synonyms:C9H8N2O2S

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Chemical Property of C9H8N2O2S
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Technology Process of C9H8N2O2S

There total 1 articles about C9H8N2O2S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With caesium carbonate; In acetone; for 14h; Heating / reflux;
Guidance literature:
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 72h; Product distribution / selectivity;
Guidance literature:
Multi-step reaction with 2 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h / 20 °C
2: dichloromethane / 18 h / 20 °C
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
upstream raw materials:

5-bromothiazol-2-amine hydrobromide

recorcinol

Downstream raw materials:

C27H26N2O8S2

C45H44N2O14S3

C29H29N3O9S2

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